磷酸三(2,2,2-三氟乙基)酯合成路线 (共 20 条)
反应条件
hydrogen fluoride; triethylamine in dichloromethane 12 h; Title compound not separated from byproducts;
参考文献
Timperley, Christopher M.; Arbon, Robert E.; Saunders, Sally A.; Waters, Matthew J.
Journal of Fluorine Chemistry, 2002 , vol. 113, # 1 p. 65 - 78
反应条件
chloral T=20°C; 72 h;
参考文献
Mironov, V.F.; Sinyashina, T.N.; Ofitserov, E.N.; Konovalova, I.V.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.2 p. 1225 - 1227
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1366 - 1368
反应条件
tetrahydrofuran; PAIBN T=30°C; 1 h; UV-irradiation;
参考文献
Nalli, Thomas W.; Stanek, Lee G.; Molenaar, Rebekka H.; Weidell, Krysia L.; Meyer, Justin P.; Johnson, Brandon R.; Steckler, Timothy T.; Wackerly, Jay Wm.; Studler, Missy Jo; Vickerman, Kevin L.; Klankowski, Stephen A.
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3561 - 3569
参考文献
Lowther, Nicholas; Crook, Polly; Hall, Dennis
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 30, p. 405 - 408
反应条件
water in toluene; acetonitrile T=31°C; H2(18)O, hydrolysis of a series of phosphoranes derived from Ar3P and ArP(OCH2CF3)2; Mechanism;
参考文献
Lowther, Nicholas; Hall, C. Dennis
Journal of the Chemical Society, Chemical Communications, 1985 , # 19 p. 1303 - 1305
参考文献
Mironov, V.F.; Sinyashina, T.N.; Ofitserov, E.N.; Konovalova, I.V.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.2 p. 1225 - 1227
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1366 - 1368
参考文献
Mironov, V.F.; Sinyashina, T.N.; Ofitserov, E.N.; Konovalova, I.V.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.2 p. 1225 - 1227
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1366 - 1368
反应条件
cyclohexane-1,2-epoxide UV-irradiation;
参考文献
Nalli, Thomas W.; Stanek, Lee G.; Molenaar, Rebekka H.; Weidell, Krysia L.; Meyer, Justin P.; Johnson, Brandon R.; Steckler, Timothy T.; Wackerly, Jay Wm.; Studler, Missy Jo; Vickerman, Kevin L.; Klankowski, Stephen A.
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3561 - 3569
反应条件
in decalin T=181.9°C; var. temp.; Rate constantKinetics;
参考文献
Lowther, Nicholas; Crook, Polly; Hall, C. Dennis
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 102, # 1-4 p. 195 - 204
反应条件
3,6,9,12-tetraoxatetradecane-1,14-diol; sodium iodide
参考文献
Krogh et al.
Journal of Organic Chemistry, 1954 , vol. 19, p. 1124