反应条件
1: 97 percent / 5percent KOH / methanol; H2O
2: NEt3 / tetrahydrofuran / 0.75 h / -10 °C
3: 59 percent / tetrahydrofuran / Ambient temperature
4: 49 percent / NaBH4, acetic acid / tetrahydrofuran / 3.5 h / Heating
5: 61 percent / PPh3, n-Bu3N / Pd(OAc)2 / hexamethylphosphoric acid triamide / 5 h / 100 °C
6: 90 percent / H2 / PtO2 / ethanol
View Scheme
参考文献
Mori, Miwako; Washioka, Yumiko; Urayama, Takao; Yoshiura, Kagari; Chiba, Katsumi; Ban, Yoshio
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4058 - 4067