N-(4-甲氧基苯基)-N-甲基乙酰胺合成路线 (共 14 条)
反应条件
sodium hydroxide in acetone 0.25 h; Heating / reflux;
参考文献
Obshestvo S Ogranichennoy Otvetstvennostiu Inoxim; Company IFO, LLC; Ivanov, Youri Alexandrovich; Frolov, Alexander Yourievich; Osinin, Valeriy Vladimirovich; Perevezentzev, Vladimir Mixaylovich
Patent: EP2014643 A1, 2009 ;
Location in patent: Page/Page column 4 ;
反应条件
sodium amide; toluene anschliessend mit Dimethylsulfat;
参考文献
O'Neill, Brian Thomas; Nagel, Arthur Adam; Humphrey, John Michael; Sobolov-Jaynes, Susan Beth; Chappie, Thomas Allen; Vincent, Lawrence Albert; Arnold, Eric Platt; Huang, Jianhua
Patent: US2003/87925 A1, 2003 ;
US 20030087925 A1
反应条件
oxygen in acetonitrile T=30°C; 5 h;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
反应条件
1: pyridine / CH2Cl2 2: NaH / tetrahydrofuran / 20 °C View Scheme
参考文献
Zhu, Manghong; Zhang, Chen; Nwachukwu, Jerome C.; Srinivasan, Sathish; Cavett, Valerie; Zheng, Yangfan; Carlson, Kathryn E.; Dong, Chune; Katzenellenbogen, John A.; Nettles, Kendall W.; Zhou, Hai-Bing
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 43 p. 8692 - 8700
反应条件
oxygen; acetic anhydride in acetonitrile T=30°C; 5 h;
参考文献
Murata, Satoru; Tamatani, Akira; Suzuki, Kaoru; Miura, Masahiro; Nomura, Masakatsu
Chemistry Letters, 1990 , # 5 p. 757 - 760
参考文献
Newkome, George R.; Yuanjiao, Xia
Heterocycles, 1983 , vol. 20, # 6 p. 981 - 982
参考文献
Thielepape
Chemische Berichte, 68<935> 751
Full Text Show Details
Uyeyanagi
Takeda Kenkyusho Nenpo, 1949 , vol. 8, p. 22,24,26
Chem.Abstr., 1953 , p. 4854
反应条件
lead(IV) acetate; chloroform
参考文献
Horner et al.
Chemische Berichte, 1959 , vol. 92, p. 288,289
反应条件
1: diethyl ether; sodium ethylate / Behandeln des Reaktionsgemisches mit konz.Schwefelsaeure 2: concentrated H2SO4 3: PCl5; POCl3 4: aqueous NaOH 5: aqueous NaOH View Scheme
参考文献
Thielepape; Fulde
Chemische Berichte, 1939 , vol. 72, p. 1432,1438
反应条件
1: diethyl ether; sodium ethylate / Behandeln des Reaktionsgemisches mit konz.Schwefelsaeure 2: concentrated H2SO4 3: PCl5; POCl3 4: SnCl2; concentrated HCl / anschliessendes Behandeln mit wss. NaOH View Scheme
参考文献
Thielepape; Fulde
Chemische Berichte, 1939 , vol. 72, p. 1432,1438