N-(4-甲氧基苯基)-N-甲基乙酰胺合成路线 （共 14 条）
反应条件
1: With sulfuric acid; water 2 h; Heating / reflux; 2: With sodium hydroxide; water Product distribution / selectivity;
参考文献
Obshestvo S Ogranichennoy Otvetstvennostiu Inoxim; Company IFO, LLC; Ivanov, Youri Alexandrovich; Frolov, Alexander Yourievich; Osinin, Valeriy Vladimirovich; Perevezentzev, Vladimir Mixaylovich
Patent: EP2014643 A1, 2009 ;
Location in patent: Page/Page column 4 ;
反应条件
1: diethyl ether; sodium ethylate / Behandeln des Reaktionsgemisches mit konz.Schwefelsaeure
2: concentrated H2SO4
3: PCl5; POCl3
4: aqueous NaOH
5: aqueous NaOH
6: ethanol; concentrated H2SO4
View Scheme
参考文献
Thielepape; Fulde
Chemische Berichte, 1939 , vol. 72, p. 1432,1438
反应条件
1: diethyl ether; sodium ethylate / Behandeln des Reaktionsgemisches mit konz.Schwefelsaeure
2: concentrated H2SO4
3: PCl5; POCl3
View Scheme
参考文献
Thielepape; Fulde
Chemische Berichte, 1939 , vol. 72, p. 1432,1438
反应条件
1: diethyl ether; sodium ethylate / Behandeln des Reaktionsgemisches mit konz.Schwefelsaeure
2: concentrated H2SO4
3: PCl5; POCl3
4: SnCl2; concentrated HCl / anschliessendes Behandeln mit wss. NaOH
5: ethanol; concentrated H2SO4
View Scheme
参考文献
Thielepape; Fulde
Chemische Berichte, 1939 , vol. 72, p. 1432,1438
