1,5-二氯六甲基三硅氧烷合成路线 (共 36 条)
反应条件
T=600°C; P=0.1 - 1 Torr; 0.00833333 h; Further byproducts given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 62, # 6.1 p. 1308 - 1313,1076 - 1081
反应条件
aluminium trichloride in neat (no solvent) ((CH3)2SiO)4 and AlCl3 at about 120°C;;
参考文献
US2645654 , ;
C. A., , p. 7050
反应条件
sodium nitrate T=0°C; 2 h; Yield givenFurther byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Russian Journal of General Chemistry, , vol. 68, # 4 p. 658 - 659
Zhurnal Obshchei Khimii, , vol. 68, # 4 p. 699 - 700
反应条件
dihydrogen hexachloroplatinate in tetrahydrofuran 3 h; Heating; Further byproducts given;
参考文献
Russian Journal of General Chemistry, , vol. 64, # 4.2 p. 568 - 569
Zhurnal Obshchei Khimii, , vol. 64, # 4 p. 623 - 625
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 806,807, 809; engl. Ausg. S. 827, 828, 830
反应条件
(benzyloxy)trichlorosilane T=600°C; P=0.1 - 1 Torr; 0.00833333 h; also octamethylcyclotetrasiloxane D4; other temp.; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 62, # 6.1 p. 1308 - 1313,1076 - 1081
反应条件
CoCl2 in acetonitrile 168 h; Ambient temperatureother acyl chlorides; also in the presence of hexamethyldisiloxane or trimethylacetoxysilane; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 62, # 1.1 p. 97 - 102,79 - 83
反应条件
triethylamine in diethyl ether 1 h; Heating;
参考文献
Sonnek, Georg; Engelbrecht, Lothar
Zeitschrift fuer Chemie (Stuttgart, Germany), 1987 , vol. 27, # 9 p. 343 - 344
反应条件
triethylamine in diethyl ether 1 h; Heating;
参考文献
Sonnek, Georg; Engelbrecht, Lothar
Zeitschrift fuer Chemie (Stuttgart, Germany), 1987 , vol. 27, # 9 p. 343 - 344
反应条件
water 1.) ether. -78 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kazoura, Samih Amine; Weber, Wolliam P.
Journal of Organometallic Chemistry, 1983 , vol. 243, # 2 p. 149 - 156