3-氯-4-羟基三氟甲苯合成路线 (共 16 条)
反应条件
in tetrachloromethane
参考文献
Shell Oil Company
Patent: US4607128 A1, 1986 ;
反应条件
hydrogenchloride in 1,4-dioxane T=0 - 20°C; 12 h;
参考文献
AMOREPACIFIC CORPORATION
Patent: WO2007/120012 A1, 2007 ;
Location in patent: Page/Page column 98 ;
WO 2007/120012 A1
反应条件
potassium hydroxide in dimethyl sulfoxide
参考文献
US4470930 A1, ;
US4582948 A1, ;
反应条件
chlorine; toluene-4-sulfonic acid in tetrachloromethane; water
反应条件
potassium hydroxide; dimethyl sulfoxide in tetrachloromethane
反应条件
sodium chlorite; sulfuric acid in water 0.5 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1861 - 1864
反应条件
sodium chlorite; sulfuric acid in water T=10°C; 0.5 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1861 - 1864
反应条件
1.1: mCPBA 1.2: hydrolysis 2.1: SO2Cl2; diisobutylamine View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 15, # 14 p. 3347 - 3351
反应条件
sulfuric acid; copper(l) chloride; sodium nitrite
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 184, # 3 p. 651 - 659
反应条件
in water pH=2.0; Photolysis; Quantum yieldProduct distribution; Further Variations:pH-valuesReagentsexcitation wavelength;
参考文献
Pest Management Science, , vol. 57, # 4 p. 372 - 379