3-苯基咪唑并[1,5-a]吡啶合成路线 (共 15 条)
反应条件
1: triethylamine / dichloromethane / 6 h / 0 - 20 °C / |Inert atmosphere 2: 2-methoxy-pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 16 h / 35 °C / |Inert atmosphere View Scheme
参考文献
Pelletier, Guillaume; Charette, Andre B.
Organic Letters, 2013 , vol. 15, # 9 p. 2290 - 2293
反应条件
1: With nickel dichloride T=20°C; Kumada-Tamao-Corriu cross-coupling; 3 h; 2: With water; ammonium chloride
参考文献
Shibahara, Fumitoshi; Yamaguchi, Eiji; Kitagawa, Asumi; Imai, Akio; Murai, Toshiaki
Tetrahedron, 2009 , vol. 65, # 26 p. 5062 - 5073
反应条件
1: 31 percent / TsCl, NEt3 / CH2Cl2 / 24 h 2: 50 percent / acetone / 2 h / Irradiation View Scheme
参考文献
Benincori, Tiziana; Brenna, Elisabetta; Sannicolo, Franco
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 6 p. 675 - 680
反应条件
2: 26 percent / PCl5, POCl3, pyridine / 4 h / 50 °C View Scheme
参考文献
Benincori, Tiziana; Brenna, Elisabetta; Sannicolo, Franco
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 6 p. 675 - 680
反应条件
2: 26 percent / PCl5, POCl3, pyridine / 4 h / 50 °C View Scheme
参考文献
Benincori, Tiziana; Brenna, Elisabetta; Sannicolo, Franco
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 6 p. 675 - 680