1-[3-(3-丁烯-1-基)苯基]乙酮合成路线 (共 3 条)
反应条件
1: 1-bromo-3-(but-3-en-1-yl)benzene With magnesium in tetrahydrofuran 2: acetic anhydride in tetrahydrofuran T=-78°C; Further stages.;
参考文献
Thalji; Ahrendt; Bergman; Ellman
Journal of the American Chemical Society, 2001 , vol. 123, # 39 p. 9692 - 9693
反应条件
1.1: 84 percent / diethyl ether; tetrahydrofuran / 2 h 2.1: magnesium / tetrahydrofuran 2.2: 67 percent / tetrahydrofuran / -78 °C View Scheme
参考文献
Thalji; Ahrendt; Bergman; Ellman
Journal of the American Chemical Society, 2001 , vol. 123, # 39 p. 9692 - 9693
反应条件
1: PdCl2(dppf) / diethyl ether / 24 h / 20 °C 2: p-TsOH / acetone / 4 h / 20 °C View Scheme
参考文献
Kuo, Chih-Wei; Fang, Jim-Min
Synthetic Communications, 2001 , vol. 31, # 6 p. 877 - 892