1,2,3,4,5,6,7,8-八丙基蒽合成路线 （共 5 条）
反应条件
silver(I) acetate; palladium diacetate in toluene T=110°C; 48 h;
参考文献
Huang, Wenying; Zhou, Xin; Kanno, Ken-Ichiro; Takahashi, Tamotsu
Organic Letters, 2004 , vol. 6, # 14 p. 2429 - 2431
反应条件
silver(I) acetate; palladium diacetate in toluene T=110°C; 48 h;
参考文献
Huang, Wenying; Zhou, Xin; Kanno, Ken-Ichiro; Takahashi, Tamotsu
Organic Letters, 2004 , vol. 6, # 14 p. 2429 - 2431
反应条件
1: (4Z,6Z)-5,6-dipropyl-4,7-diiododeca-4,6-diene With tert.-butyl lithium in tetrahydrofuran; pentane T=-78 - 20°C; 1 h; Inert atmosphere; 2: 1,2,3,4-tetrapropyl-6,7-diiodonaphthalene With N,N'-dimethyl-N,N'-propyleneurea; copper(l) chloride in tetrahydrofuran; pentane T=50°C; Inert atmosphere;
参考文献
Zhou, Lishan; Nakajima, Kiyohiko; Kanno, Ken-ichiro; Takahashi, Tamotsu
Tetrahedron Letters, 2009 , vol. 50, # 23 p. 2722 - 2726
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine; methyl iodide in hexane T=20 - 50°C; 4 h; Product distribution; Further Variations:Reagents;
参考文献
Kitamura, Masanori; Shen, Baojian; Liu, Yanjun; Zheng, Hegen; Takahashi, Tamotsu
Chemistry Letters, 2001 , # 7 p. 646 - 647
反应条件
hydrogenchloride; n-butyllithium
参考文献
Takahashi, Tamotsu
Patent: US2003/116755 A1, 2003 ;
