2,3-二甲氧基-1,3-丁二烯合成路线 （共 31 条）
反应条件
und Behandeln des Reaktionsprodukts mit wss.-alkoh.NaOCl-Loesung;
参考文献
Johnson; Jobling; Bodamer
Journal of the American Chemical Society, 1941 , vol. 63, p. 135
反应条件
T=0°C; 6 h; Neat (no solvent);
参考文献
MroB, Gerson; Langer, Peter
Letters in Organic Chemistry, 2009 , vol. 6, # 3 p. 189 - 190
反应条件
ozone in pentane
T=-30°C;
参考文献
Griesbaum, Karl; Kim, Woo-Sun
Journal of Organic Chemistry, 1992 , vol. 57, # 21 p. 5574 - 5577
反应条件
ozone in methanol
T=-30°C;
参考文献
Griesbaum, Karl; Kim, Woo-Sun
Journal of Organic Chemistry, 1992 , vol. 57, # 21 p. 5574 - 5577
参考文献
Griesbaum, Karl; Kim, Woo-Sun
Journal of Organic Chemistry, 1992 , vol. 57, # 21 p. 5574 - 5577
反应条件
in ethylene glycol dimethyl ether
T=180°C; Diels-Alder reaction; 120 h;
参考文献
Fujita, Reiko; Yoshisuji, Toshiteru; Wakayanagi, Sota; Wakamatsu, Hideaki; Matsuzaki, Hisao
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 2 p. 204 - 208
反应条件
in toluene
T=140°C; 40 h;
参考文献
Reichwagen, Jens; Hopf, Henning; Del Guerzo, Andre; Belin, Colette; Bouas-Laurent, Henri; Desvergne, Jean-Pierre
Organic Letters, 2005 , vol. 7, # 6 p. 971 - 974
反应条件
1: 2.) KOH / 1.) toluene, reflux, 20 h, 2.) CH2Cl2, MeOH
2: 85 percent / NaBH4 / propan-2-ol / Heating
View Scheme
参考文献
Pozzo, Jean-Luc; Clavier, Gilles M.; Colomes, Michel; Bouas-Laurent, Henri
Tetrahedron, 1997 , vol. 53, # 18 p. 6377 - 6390
反应条件
perchloric acid in water
T=25°C; 0.0333333 h; Rate constantMechanism;
参考文献
Kresge, A. Jerry; Yin, Ya
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1753 - 1756
反应条件
in o-xylene
T=180°C; Diels-Alder reaction; 72 h;
参考文献
Fujita, Reiko; Yoshisuji, Toshiteru; Wakayanagi, Sota; Wakamatsu, Hideaki; Matsuzaki, Hisao
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 2 p. 204 - 208
