2-氯-1,1-二氟乙烯合成路线 （共 69 条）
反应条件
1: 1,1,1-trifluoro-2-chloroethane With zinc(II) chloride in tetrahydrofuran T=20°C; 2 h; 2: 4'-iodoacetophenone With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=65°C; 3 h; Title compound not separated from byproducts;
参考文献
Anilkumar; Burton, Donald J.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 5 p. 835 - 843
反应条件
Catalyst M-Chromium oxide; hydrogen fluoride T=380°C; 2.77778E-06 h; var. H : Cr ratios; Product distribution;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 4 p. 374 - 375
反应条件
potassium hydroxide T=280°C; P=83600 Torr; 13 h;
参考文献
Wu, Kai; Chen, Qing-Yun
Journal of Fluorine Chemistry, 2002 , vol. 113, # 1 p. 79 - 83
反应条件
ethanol; iron; zinc T=130 - 135°C;
反应条件
1: With hydrogen fluoride; chromium - based fluorination catalyst T=180°C; 2: With Cr and In on graphite catalyst T=180°C; 4 h; Inconel 600 type reactor; 3: With Cr on active alumina catalyst Inconel 600 type reactor; Product distribution / selectivity;
参考文献
WO2005/92823 A2, ;
Page/Page column 10-16 ;
参考文献
Stepanov; Delyagina; Cherstkov
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 9 p. 1290 - 1295
参考文献
Russian Journal of Organic Chemistry, , vol. 46, # 9 p. 1290 - 1295
反应条件
Catalyst M-Chromium oxide in gas T=249.9°C; 0.000833333 h; various temp.; ΔRH0; ΔRG0; Product distributionThermodynamic data;
参考文献
Journal of Fluorine Chemistry, , vol. 75, # 1 p. 103 - 110
反应条件
hydrogen fluoride; Catalyst M-Chromium oxide in gas T=249.9°C; 0.000833333 h; various temp.; ΔRH0; ΔRG0; Product distributionThermodynamic data;
参考文献
Journal of Fluorine Chemistry, , vol. 75, # 1 p. 103 - 110
参考文献
Industrial and Engineering Chemistry, , vol. 43, p. 1253,1254
