1-氯-1,1,2,3,3,3-六氟丙烷合成路线 （共 9 条）
反应条件
hydrogenchloride; hydrogen fluoride; 98percentChromium/2percentPalladium Catalyst (calcined at 900 C) T=100 - 400°C; P=760.051 Torr; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/79265 A1, 2008 ;
Location in patent: Page/Page column 12-14 ;
反应条件
chlorine T=23°C; Photochlorination; P=760.051 Torr; 1 h; Irradiation with sunlamp; Product distribution / selectivity;
参考文献
Rao, Velliyur Nott Mallikarjuna; Sievert, Allen Capron
Patent: US2007/265368 A1, 2007 ;
Location in patent: Page/Page column 5 ;
反应条件
hydrogen fluoride; hydrogen T=300 - 350°C; P=760.051 Torr; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/2501 A2, 2008 ;
Location in patent: Page/Page column 14 ;
反应条件
(NH4)2S2O8; ammonium formate in N,N-dimethyl-formamide T=30 - 40°C;
参考文献
Hu, Chang-Ming; Tu, Ming-Hu
Journal of Fluorine Chemistry, 1991 , vol. 55, # 1 p. 105 - 108
反应条件
hydrogen fluoride; 1percent Pd supported on fluorided alumina catalyst T=125 - 300°C; P=760.051 Torr; 0.00833333 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2005/37742 A1, 2005 ;
Location in patent: Page/Page column 16; 19 ;
参考文献
Haszeldine, Robert N.; Rowland, Ronald; Tipping, Anthony E.; Tyrrell, Geoffrey
Journal of Fluorine Chemistry, 1982 , vol. 21, p. 253 - 260
参考文献
Haszeldine, Robert N.; Rowland, Ronald; Tipping, Anthony E.; Tyrrell, Geoffrey
Journal of Fluorine Chemistry, 1982 , vol. 21, p. 253 - 260
反应条件
T=290°C; 96 h; Further byproducts given;
参考文献
Haszeldine, Robert N.; Rowland, Ronald; Tipping, Anthony E.; Tyrrell, Geoffrey
Journal of Fluorine Chemistry, 1982 , vol. 21, p. 253 - 260
反应条件
triethylsilane; meta-chloroperoxybenzoic acid 1) 25 deg C, 1 h, 2) 100 deg C, 12 h; Yield givenYields of byproduct given;
参考文献
Petrov, Viacheslav A.
Journal of Organic Chemistry, 1998 , vol. 63, # 21 p. 7294 - 7297
