N,N-双(三氟甲基)羟胺合成路线 （共 120 条）
反应条件
sodium hydride 1.) Et2O, -78 deg C, 0.5 h, 2.) diglyme, 50 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ducker, Graham E.; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 1-2 p. 133 - 138
参考文献
Haszeldine; Mattinson
Journal of the Chemical Society, 1957 , p. 1741,1745
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
fluorine; cesium fluoride in monofluoro-trichloromethane T=-78°C; Fluorination; 24 h; Further byproducts given;
参考文献
Minkwitz, Rolf; Reinemann, Stefan; Ludwig, Ralf
Journal of Fluorine Chemistry, 1999 , vol. 99, # 2 p. 145 - 149
反应条件
fluorine; cesium fluoride in monofluoro-trichloromethane T=-78°C; Fluorination; 24 h; Further byproducts given;
参考文献
Minkwitz, Rolf; Reinemann, Stefan; Ludwig, Ralf
Journal of Fluorine Chemistry, 1999 , vol. 99, # 2 p. 145 - 149
反应条件
benzyl azide in tetrachloromethane
T=20°C; 0.5 h;
参考文献
Banks, Ronald E.; Birchall, J. Michael; Haszeldine, Robert N.; Hughes, Raymond A.; Nona, Shmaiel N.; Stephens, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 455 - 456
反应条件
hydrogenchloride
T=60°C; 24 h;
参考文献
ANG, H. G.; SO, K. K.
Journal of Fluorine Chemistry, 1985 , vol. 27, p. 451 - 460
反应条件
arsenic trihydride
T=-126 - 20°C;
参考文献
Ang, H. G.; Koh, C. H.
Journal of Fluorine Chemistry, 1992 , vol. 58, # 1 p. 9 - 15
反应条件
N,N-bis(trifluoromethyl)nitroxide
T=20°C; 0.5 h;
参考文献
Banks, Ronald E.; Birchall, J. Michael; Haszeldine, Robert N.; Hughes, Raymond A.; Nona, Shmaiel N.; Stephens, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 455 - 456
参考文献
Ang, H. G.; Lien, W. S.
Journal of Fluorine Chemistry, 1980 , vol. 15, p. 453 - 470
