2,2-二丁基-[1,3,2]二氧锡合成路线 （共 23 条）
反应条件
in toluene T=110 - 114°C; 5 h;
参考文献
JANSSEN PHARMACEUTICA NV
Patent: WO2008/58902 A2, 2008 ;
Location in patent: Page/Page column 7-8 ;
反应条件
ethylene glycol in toluene byproducts: H2O; azeotropic dehydration;
参考文献
Davies, Alwyn G.; Price, Allan J.
Journal of Organometallic Chemistry, 1983 , vol. 258, # 1 p. 7 - 14
反应条件
in cyclohexane refluxing (2 h, azeotropic water removal), evapn., washing (EtOH); crystn. (toluene), drying (vac., 60°C);
参考文献
Deleuze, H.; Maillard, B.
Journal of Organometallic Chemistry, 1995 , vol. 490, # 1-2 p. C14 - C17
反应条件
byproducts: (CH3O)2CO; 185°C; 2 h;
参考文献
Sakai et al.
Journal of the Chemical Society, Chemical Communications, 1975 , p. 265
反应条件
in dichloromethane attempted recrystn. from CH2Cl2; identified by m.p.;
参考文献
Davies, Alwyn G.; Hawari, Jalal A.-A.; Hua-De, Pan
Journal of Organometallic Chemistry, 1983 , vol. 251, # 2 p. 203 - 208
反应条件
1: pentane View Scheme
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.2, page 56 - 60
反应条件
1: benzene View Scheme
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.2, page 56 - 60
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.2, page 56 - 60
参考文献
Sakai et al.
Journal of the Chemical Society, Chemical Communications, 1975 , p. 265
Full Text View citing articles Show Details
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.4, page 61 - 63
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.2, page 56 - 60
