2,2-二丁基-[1,3,2]二氧锡合成路线 (共 23 条)
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.2, page 56 - 60
参考文献
Journal of Organometallic Chemistry, , vol. 256, # 2 p. 251 - 260
反应条件
1.) CHCl3, 5-7 deg C; 2.) CHCl3, r.t.; Multistep reaction;
参考文献
Roelens, Stefano
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1617 - 1626
反应条件
in cyclohexane N2-atmosphere; dropwise addn. of excess borane complex in THF (15 min, room temp.), stirring (1-3 h), addn. of water, drying (MgSO4); evapn., distn.;
参考文献
Deleuze, H.; Maillard, B.
Journal of Organometallic Chemistry, 1995 , vol. 490, # 1-2 p. C14 - C17
反应条件
1: toluene 2: tetrachloromethane View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 251, # 2 p. 203 - 208
参考文献
Davies, Alwyn G.; Hua-De, Pan; Hawari, Jalal A. -A.
Journal of Organometallic Chemistry, 1983 , vol. 256, # 2 p. 251 - 260
反应条件
1.) CHCl3, 5-7 deg C; 2.) CHCl3, r.t.; Multistep reaction;
参考文献
Roelens, Stefano
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1617 - 1626
反应条件
in benzene
T=80°C; 1 h; Further byproducts given;
参考文献
Roelens, Stefano
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1617 - 1626
反应条件
in benzene
Heatingovernight;
参考文献
Podda, Gianni; Anchisi, Carlo; Corda, Luciana; Fadda, Anna Maria
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1789 - 1791
参考文献
Roelens, Stefano
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1617 - 1626