1: With benzo[1,3,2]dioxaborole; rhodium complex 2 in toluene T=20°C; Addition; Hydroboration; 2 h; 2: With sodium hydroxide; water; dihydrogen peroxide in toluene T=20°C; Oxidation; 2 h; Title compound not separated from byproducts;
参考文献
Doucet, Henri; Fernandez, Elena; Layzell, Timothy P.; Brown, John M.
Chemistry - A European Journal, 1999 , vol. 5, # 4 p. 1320 - 1330
AlMSU-F-template; NaOH in sodium hydroxide aq. NaOH; MSU-F silica wetted with furfuryl alcohol, polymerized at 85 ° C for 24 h, resulting composite heated at 850 °C for 3 h under N2, AlMSU-F template dissolved using NaOH at 100 ° C;
