乐果(有机磷杀虫、杀螨剂)-D6合成路线 （共 10 条）
反应条件
1: With sulfuric acid; sodium nitrite in water T=0°C; Diazotization; 0.583333 h; 2: With sulfuric acid Hydrolysis; oxidation; Heating; Title compound not separated from byproducts;
参考文献
Mukawa, Takashi; Inoue, Yukihiko; Shiraishi, Shinsaku
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 11 p. 2549 - 2556
反应条件
copper(I) oxide; sodium hydroxide T=250°C;
参考文献
Dow Chem. Co.
Patent: US2207753 , 1937 ;
反应条件
aluminium trichloride
参考文献
Dewar,M.J.S.; Puttnam,N.A.
Journal of the Chemical Society, 1960 , p. 959 - 963
反应条件
aluminium trichloride T=149.9°C; 173 h; other catalyst (AlBr3), temperature, time, ΔHr, ΔSr; Thermodynamic dataEquilibrium constantProduct distribution;
参考文献
Nesterova, T. N.; Pilyshchikov, V. A.; Rozhnov, A. M.
J. Appl. Chem. USSR (Engl. Transl.), 1983 , vol. 56, # 6 p. 1338 - 1342,1257 - 1261
反应条件
aluminum tri-bromide T=169.9°C; 33 h; other catalyst (AlCl3), temperature, time, ΔHr, ΔSr; Thermodynamic dataEquilibrium constantProduct distribution;
参考文献
Nesterova, T. N.; Pilyshchikov, V. A.; Rozhnov, A. M.
J. Appl. Chem. USSR (Engl. Transl.), 1983 , vol. 56, # 6 p. 1338 - 1342,1257 - 1261
反应条件
Houdry HA-100 alumina T=300°C; Product distributionMechanism;
参考文献
Klemm, LeRoy H.; Taylor, Dennis R.
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4326 - 4329
反应条件
Houdry HA-100 alumina T=300°C; Product distributionMechanism;
参考文献
Klemm, LeRoy H.; Taylor, Dennis R.
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4326 - 4329
反应条件
Houdry HA-100 alumina T=350°C; other substrates; other temperatures and concentrations; Product distributionMechanism;
参考文献
Klemm, LeRoy H.; Taylor, Dennis R.
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4326 - 4329
反应条件
aluminium trichloride T=149.9°C; 173 h; other catalyst (AlBr3), temperature, time, ΔHr, ΔSr; Thermodynamic dataEquilibrium constantProduct distribution;
参考文献
Nesterova, T. N.; Pilyshchikov, V. A.; Rozhnov, A. M.
J. Appl. Chem. USSR (Engl. Transl.), 1983 , vol. 56, # 6 p. 1338 - 1342,1257 - 1261
反应条件
aluminium trichloride
T=169.9°C; 10 h; other catalyst (AlBr3), temperature, time, ΔHr, ΔSr; Thermodynamic dataEquilibrium constantProduct distribution;
参考文献
Nesterova, T. N.; Pilyshchikov, V. A.; Rozhnov, A. M.
J. Appl. Chem. USSR (Engl. Transl.), 1983 , vol. 56, # 6 p. 1338 - 1342,1257 - 1261
