5-溴-2-甲基苯甲酸乙酯合成路线 （共 3 条）
反应条件
1: With hydrogen bromide in water Cooling with ice; 2: With hydrogen bromide; sodium nitrite in water 3: With hydrogen bromide; copper(I) bromide in water T=70°C; Cooling with ice;
参考文献
The Government of the United States of America, as represented by the Secretary, Department of HHS; Albany Molecular Research, Inc.; Science Applications International Corporation
Patent: US2009/312323 A1, 2009 ;
Location in patent: Page/Page column 13 ;
反应条件
sulfuric acid in benzene Cooling with iceReflux;
参考文献
Shi, Yongheng; Zhao, Guilong; Lou, Yuanyuan; Wang, Yuli; Shao, Hua; Liu, Wei; Xu, Weiren; Tang, Lida
Chinese Journal of Chemistry, 2011 , vol. 29, # 6 p. 1192 - 1198
反应条件
copper(l) iodide; sodium iodide; N-methyl-2-(methylamino)ethylamine
T=110°C; 15 h; Inert atmosphere;
参考文献
GREEN CROSS CORPORATION; LEE, Jinhwa; KIM, Jeongmin; LEE, Suk Ho; LEE, Junwon; SONG, Kwang-Seop; PARK, Eun-Jung; KIM, Min Ju; SEO, Hee Jeong; LEE, Sung-Han; SON, Eun Jung; KIM, Jong Yup; KANG, Suk Youn; KONG, Younggyu
Patent: WO2011/159067 A2, 2011 ;
Location in patent: Page/Page column 50-51 ;
WO 2011/159067 A2
