二(4-氯-3-硝基苯基)二硫醚合成路线 （共 7 条）
反应条件
sodium disulfite; potassium iodide in water; butanone Heatingother reagent: hydriodic acid;
参考文献
Lynch, Doreen C.; Miller, James R.; Spawn, Terence D.
Synthetic Communications, 1997 , vol. 27, # 5 p. 897 - 905
反应条件
1: phosphorous oxychloride, sulfolane / acetonitrile / 0.67 h / 70 °C 2: 92.6 percent / potassium iodide, sodium metabisulfite / butan-2-one; H2O / Heating; other reagent: hydriodic acid View Scheme
参考文献
Lynch, Doreen C.; Miller, James R.; Spawn, Terence D.
Synthetic Communications, 1997 , vol. 27, # 5 p. 897 - 905
反应条件
silver(II) fluoride; copper in various solvent(s) T=60 - 130°C; 5 h;
参考文献
Sipyagin, Alexey M.; Enshov, Vyacheslav S.; Kashtanov, Sergei A.; Bateman, Colin P.; Mullen, Brian D.; Tan, Ying-Teck; Thrasher, Joseph S.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 9 p. 1305 - 1316
反应条件
1: With silver(II) fluoride; copper in various solvent(s) T=60 - 130°C; 5 h; 2: T=220 - 225°C; 1.5 h;
参考文献
Sipyagin, Alexey M.; Enshov, Vyacheslav S.; Kashtanov, Sergei A.; Bateman, Colin P.; Mullen, Brian D.; Tan, Ying-Teck; Thrasher, Joseph S.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 9 p. 1305 - 1316
反应条件
sodium sulfide; sodium hydroxide Behandeln des Reaktionsgemisches mit Dimethylsulfat;
参考文献
Bourquin et al.
Helvetica Chimica Acta, 1959 , vol. 42, p. 2541,2543
参考文献
Tanaka,K. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 536 - 539
反应条件
sodium sulfide Yield given. Multistep reaction;
参考文献
Lynch, Doreen C.; Miller, James R.; Spawn, Terence D.
Synthetic Communications, 1997 , vol. 27, # 5 p. 897 - 905
