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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
359784-28-4
合成路线
（共 10 条）
186581-53-3
重氮甲烷
+
359784-27-3
→
反应条件
359784-28-4
反应条件
in diethyl ether T=0 - 15°C; 3 h;
参考文献
Liu, Ying; Feng, Yabing; Wang, Renxiao; Gao, Ying; Lai, Luhua
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1639 - 1641
6340-55-2
2-氯-6-甲氧基-4-甲基-喹啉
→
反应条件
359784-28-4
反应条件
1: 80.8 percent / KOH / 4 h / 160 °C 2: 20.1 percent / ZnCl2 / 3 h / 160 °C 3: 74.6 percent / OsO4; NaIO4 / 24 h / 24 - 26 °C 4: 95.6 percent / AgNO3; NaOH / 12 h / 20 °C 5: 100 percent / (COCl)2 / 24 h / 20 °C 6: 92 percent / diethyl ether / 3 h / 0 - 15 °C View Scheme
参考文献
Liu, Ying; Feng, Yabing; Wang, Renxiao; Gao, Ying; Lai, Luhua
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1639 - 1641
5342-23-4
4-甲基-2-羟基-6-甲氧基喹啉
→
反应条件
359784-28-4
反应条件
1: 89.3 percent / POCl3 / 0.5 h / 110 - 120 °C 2: 80.8 percent / KOH / 4 h / 160 °C 3: 20.1 percent / ZnCl2 / 3 h / 160 °C 4: 74.6 percent / OsO4; NaIO4 / 24 h / 24 - 26 °C 5: 95.6 percent / AgNO3; NaOH / 12 h / 20 °C 6: 100 percent / (COCl)2 / 24 h / 20 °C 7: 92 percent / diethyl ether / 3 h / 0 - 15 °C View Scheme
参考文献
Liu, Ying; Feng, Yabing; Wang, Renxiao; Gao, Ying; Lai, Luhua
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1639 - 1641
359784-21-7
→
反应条件
359784-28-4
反应条件
1: 20.1 percent / ZnCl2 / 3 h / 160 °C 2: 74.6 percent / OsO4; NaIO4 / 24 h / 24 - 26 °C 3: 95.6 percent / AgNO3; NaOH / 12 h / 20 °C 4: 100 percent / (COCl)2 / 24 h / 20 °C 5: 92 percent / diethyl ether / 3 h / 0 - 15 °C View Scheme
参考文献
Liu, Ying; Feng, Yabing; Wang, Renxiao; Gao, Ying; Lai, Luhua
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1639 - 1641
5437-98-9
乙酰基乙酰对甲氧基苯胺
→
反应条件
359784-28-4
反应条件
1: 62.4 percent / H2SO4 / 2 h / 90 - 110 °C 2: 89.3 percent / POCl3 / 0.5 h / 110 - 120 °C 3: 80.8 percent / KOH / 4 h / 160 °C 4: 20.1 percent / ZnCl2 / 3 h / 160 °C 5: 74.6 percent / OsO4; NaIO4 / 24 h / 24 - 26 °C 6: 95.6 percent / AgNO3; NaOH / 12 h / 20 °C 7: 100 percent / (COCl)2 / 24 h / 20 °C 8: 92 percent / diethyl ether / 3 h / 0 - 15 °C View Scheme
参考文献
Liu, Ying; Feng, Yabing; Wang, Renxiao; Gao, Ying; Lai, Luhua
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1639 - 1641
104-94-9
对甲氧基苯胺
→
反应条件
359784-28-4
反应条件
1: 73.8 percent / 0.5 h / 140 °C 2: 62.4 percent / H2SO4 / 2 h / 90 - 110 °C 3: 89.3 percent / POCl3 / 0.5 h / 110 - 120 °C 4: 80.8 percent / KOH / 4 h / 160 °C 5: 20.1 percent / ZnCl2 / 3 h / 160 °C 6: 74.6 percent / OsO4; NaIO4 / 24 h / 24 - 26 °C 7: 95.6 percent / AgNO3; NaOH / 12 h / 20 °C 8: 100 percent / (COCl)2 / 24 h / 20 °C 9: 92 percent / diethyl ether / 3 h / 0 - 15 °C View Scheme
参考文献
Liu, Ying; Feng, Yabing; Wang, Renxiao; Gao, Ying; Lai, Luhua
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1639 - 1641
359784-25-1
→
反应条件
359784-28-4
反应条件
1: 95.6 percent / AgNO3; NaOH / 12 h / 20 °C 2: 100 percent / (COCl)2 / 24 h / 20 °C 3: 92 percent / diethyl ether / 3 h / 0 - 15 °C View Scheme
参考文献
Liu, Ying; Feng, Yabing; Wang, Renxiao; Gao, Ying; Lai, Luhua
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1639 - 1641
359784-26-2
→
反应条件
359784-28-4
反应条件
1: 100 percent / (COCl)2 / 24 h / 20 °C 2: 92 percent / diethyl ether / 3 h / 0 - 15 °C View Scheme
参考文献
Liu, Ying; Feng, Yabing; Wang, Renxiao; Gao, Ying; Lai, Luhua
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1639 - 1641
359784-23-9
→
反应条件
359784-28-4
反应条件
1: 74.6 percent / OsO4; NaIO4 / 24 h / 24 - 26 °C 2: 95.6 percent / AgNO3; NaOH / 12 h / 20 °C 3: 100 percent / (COCl)2 / 24 h / 20 °C 4: 92 percent / diethyl ether / 3 h / 0 - 15 °C View Scheme
参考文献
Liu, Ying; Feng, Yabing; Wang, Renxiao; Gao, Ying; Lai, Luhua
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1639 - 1641
108-95-2
苯酚
→
反应条件
359784-28-4
反应条件
1: 80.8 percent / KOH / 4 h / 160 °C 2: 20.1 percent / ZnCl2 / 3 h / 160 °C 3: 74.6 percent / OsO4; NaIO4 / 24 h / 24 - 26 °C 4: 95.6 percent / AgNO3; NaOH / 12 h / 20 °C 5: 100 percent / (COCl)2 / 24 h / 20 °C 6: 92 percent / diethyl ether / 3 h / 0 - 15 °C View Scheme
参考文献
Liu, Ying; Feng, Yabing; Wang, Renxiao; Gao, Ying; Lai, Luhua
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 13 p. 1639 - 1641
