1,2-二氢-2-氧代-5-苯基-3-吡啶甲腈合成路线 （共 5 条）
反应条件
sodium methylate in methanol T=20°C; 5 h; Reflux;
参考文献
Zhang, Zhichao; Liu, Chengwu; Li, Xiangqian; Song, Ting; Wu, Zhiyong; Liang, Xiaomeng; Zhao, Yan; Shen, Xiaoyun; Chen, Hongbo
European Journal of Medicinal Chemistry, 2013 , vol. 60, p. 410 - 420
反应条件
1: trichlorophosphate / 3 h / 80 °C 2: sodium methylate / methanol / 5 h / 20 °C / |Reflux View Scheme
参考文献
Zhang, Zhichao; Liu, Chengwu; Li, Xiangqian; Song, Ting; Wu, Zhiyong; Liang, Xiaomeng; Zhao, Yan; Shen, Xiaoyun; Chen, Hongbo
European Journal of Medicinal Chemistry, 2013 , vol. 60, p. 410 - 420
反应条件
in sodium hydroxide; sulfuric acid
参考文献
American Cyanamid Company
Patent: US4209626 A1, 1980 ;
Title/Abstract Full Text Show Details
American Cyanamid Company
Patent: US4242515 A1, 1980 ;
反应条件
phosphorus pentachloride; trichlorophosphate T=20°C; 1 h; Heating / reflux;
参考文献
Garland, Stephen; Haigh, David; Hickey, Deidre Mary Bernadette; Liddle, John; Smith, David Glynn; Ward, Robert William; Witherington, Jason
Patent: US2004/19052 A1, 2004 ;
Location in patent: Page/Page column 16 ;
反应条件
trichlorophosphate in water
参考文献
FMC Corporation
Patent: US5532370 A1, 1996 ;
