2-甲基-4,6-二(苯基)-1,3,5-三嗪合成路线 （共 32 条）
反应条件
sodium methylate in methanol T=20 - 25°C; 504 h;
参考文献
Smolii, O. B.; Brovarets, V. S.; Drach, B. S.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 8.1 p. 1766 - 1768,1571 - 1573
反应条件
sodium methylate in ethanol Ambient temperature;
参考文献
Lin, Yang-i; Fields, Thomas L.; Lee, Ving J.; Lang, S. A.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 613 - 615
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform 2 h; Reflux;
参考文献
Brough, Peter; Gambarelli, Serge; Jacquot, Jean-Francois; Grand, Andre; Pecaut, Jacques; Rey, Paul
Chemistry - A European Journal, 2011 , vol. 17, # 40 p. 11250 - 11257
反应条件
sodium hydride in ethylene glycol dimethyl ether 24 h; Ambient temperature;
参考文献
Lorente, Antonio; Gamez, Pedro; Mar Contreras, Maria del
Heterocycles, 1994 , vol. 38, # 1 p. 113 - 124
反应条件
1: 67 percent / acetone / -10 °C 2: Et3N, cyanuric chloride / CH2Cl2 / < 0 deg C 3: 0.11 g / CHCl3 / Heating View Scheme
参考文献
Goerdeler, Joachim; Eggers, Wolfgang
Chemische Berichte, 1986 , vol. 119, # 12 p. 3737 - 3748
反应条件
1: Et3N, cyanuric chloride / CH2Cl2 / < 0 deg C 2: 0.11 g / CHCl3 / Heating View Scheme
参考文献
Goerdeler, Joachim; Eggers, Wolfgang
Chemische Berichte, 1986 , vol. 119, # 12 p. 3737 - 3748
反应条件
1: 90 percent / H2S / acetic acid / Ambient temperature 2: 97 percent / K2CO3 / acetonitrile / 60 °C 3: 70 percent / Sodium methoxide / ethanol / Ambient temperature View Scheme
参考文献
Lin, Yang-i; Fields, Thomas L.; Lee, Ving J.; Lang, S. A.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 613 - 615
反应条件
1: 97 percent / K2CO3 / acetonitrile / 60 °C 2: 70 percent / Sodium methoxide / ethanol / Ambient temperature View Scheme
参考文献
Lin, Yang-i; Fields, Thomas L.; Lee, Ving J.; Lang, S. A.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 613 - 615
反应条件
sodium methylate in methanol T=20 - 25°C; 504 h; other substrates; Mechanism;
参考文献
Smolii, O. B.; Brovarets, V. S.; Drach, B. S.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 8.1 p. 1766 - 1768,1571 - 1573
反应条件
1: 2.) aq. NaClO4 / 1.) acetone, 20-25 deg C, 2 h, 2: 25 percent / methanol / 1 h / Heating View Scheme
参考文献
Brovarets, V. S.; Vydzhak, R. N.; Drach, B. S.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 6.2 p. 1423 - 1424,1170 - 1171
