3-氯-4'-甲氧基苯丙酮合成路线 （共 8 条）
反应条件
aluminium trichloride in 1,2-dichloro-ethane T=20°C; Friedel-Crafts acylation; 3 h;
参考文献
Stephan, Holger; Geipel, Gerhard; Bernhard, Gert; Comba, Peter; Rajaraman, Gopalan; Hahn, Uwe; Voegtle, Fritz
European Journal of Inorganic Chemistry, 2005 , # 22 p. 4501 - 4508
反应条件
phosphorus trichoride Durch Behandeln des hergestellten Saeurechlorids mit Anisol und AlCl3 in Schwefelkohlenstoff;
参考文献
Journal of the Chemical Society, , p. 299,301
Chemische Berichte, , vol. 69, p. 16,17
Journal of the American Chemical Society, , vol. 67, p. 1466
Canadian Journal of Research, , vol. 8, p. 440,444
Recueil des Travaux Chimiques des Pays-Bas, , vol. 67, p. 998,1002
反应条件
potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,4-dioxane T=60°C; 20 h; Inert atmosphere;
参考文献
Jiang, Quanbin; Guo, Tenglong; Wang, Qingfu; Wu, Ping; Yu, Zhengkun
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1874 - 1880
反应条件
diarsenic pentoxide; phosphoric acid
T=140°C; modified Skraup reaction; 1 h;
参考文献
Stephan, Holger; Geipel, Gerhard; Bernhard, Gert; Comba, Peter; Rajaraman, Gopalan; Hahn, Uwe; Voegtle, Fritz
European Journal of Inorganic Chemistry, 2005 , # 22 p. 4501 - 4508
反应条件
1: 56 percent / aq. As2O5; cc. H3PO4 / 1 h / 140 °C
2: 89 percent / tin(II)chloride dihydrate / ethanol / 4 h / Heating
3: 67 percent / aq. As2O5; cc. H3PO4 / 1 h / 140 °C
View Scheme
参考文献
Alford, Peter C.; Cook, Michael J.; Lewis, Anthony P.; McAuliffe, Glenn S. G.; Skarda, Vladimir; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 705 - 710
反应条件
phosphoric acid; orthoarsenic acid
T=100 - 140°C;
参考文献
Alford, Peter C.; Cook, Michael J.; Lewis, Anthony P.; McAuliffe, Glenn S. G.; Skarda, Vladimir; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 705 - 710
反应条件
phosphoric acid; orthoarsenic acid
T=100 - 140°C;
参考文献
Alford, Peter C.; Cook, Michael J.; Lewis, Anthony P.; McAuliffe, Glenn S. G.; Skarda, Vladimir; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 705 - 710
参考文献
Profft et al.
Journal fuer Praktische Chemie (Leipzig), 1955 , vol. <4> 1, p. 57,77
