2-(三氟甲基)-3,3,3-三幅丙酸甲酯合成路线 （共 16 条）
反应条件
sulfuric acid; silica gel T=65 - 90°C; 1 h;
参考文献
Misaki, Susumu; Takamatsu, Shuichi
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 531 - 534
反应条件
sulfuric acid 0.25 h; Heating;
参考文献
Tetrahedron, , vol. 24, p. 1341 - 1356
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 21, p. 2441 - 2445
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 21, # 11 p. 2510 - 2516
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 26, p. 1023 - 1027
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 26, p. 1117 - 1121
反应条件
T=20°C; 18 h; Title compound not separated from byproducts;
参考文献
Volkonsky,A.Y.; Rokhlin,E.M.
Journal of Fluorine Chemistry, 1984 , vol. 26, p. 183
反应条件
triethylamine in 1,2,2-trifluoro-trichloroethane T=50°C; 2 h;
参考文献
Yagupol'skii, Yu. L.; Soloshonok, V. A.; Gerus. I. I.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 9 p. 1640 - 1646
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 9 p. 1828 - 1934
反应条件
triethylamine in 1,2,2-trifluoro-trichloroethane T=50°C; 2 h;
参考文献
Yagupol'skii, Yu. L.; Soloshonok, V. A.; Gerus. I. I.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 9 p. 1640 - 1646
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 9 p. 1828 - 1934
反应条件
in 1,2,2-trifluoro-trichloroethane T=20°C; 0.5 h;
参考文献
Yagupol'skii, Yu. L.; Soloshonok, V. A.; Gerus. I. I.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 9 p. 1640 - 1646
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 9 p. 1828 - 1934
反应条件
in 1,2,2-trifluoro-trichloroethane T=50°C; 3 h;
参考文献
Yagupol'skii, Yu. L.; Soloshonok, V. A.; Gerus. I. I.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 9 p. 1640 - 1646
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 9 p. 1828 - 1934
参考文献
Aktaev,N.P. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, p. 1023 - 1027
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, p. 1117 - 1121
