2-(三氟甲基)-3,3,3-三幅丙酸甲酯合成路线 （共 16 条）
参考文献
Aktaev,N.P. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, p. 1023 - 1027
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, p. 1117 - 1121
反应条件
triethylamine boron trifluoride 3 h; Heating;
参考文献
Sanders, Daniel P.; Connor, Eric F.; Grubbs, Robert H.; Hung, Raymond J.; Osborn, Brian P.; Chiba, Takashi; MacDonald, Scott A.; Grant Willson; Conley, Will
Macromolecules, 2003 , vol. 36, # 5 p. 1534 - 1542
反应条件
1: Et3N
2: methanol; H2O
View Scheme
参考文献
Aktaev,N.P. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, p. 1023 - 1027
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, p. 1117 - 1121
反应条件
(C2H5)3N*BF3 in benzene
0.666667 h; Heating; Yields of byproduct given;
参考文献
Andreev, V. G.
Russian Chemical Bulletin, 1994 , vol. 43, # 7 p. 1209 - 1213
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 7 p. 1273 - 1277
反应条件
lithium aluminium tetrahydride in diethyl ether
T=-15 - -10°C; 2.5 h;
参考文献
Misaki, Susumu; Takamatsu, Shuichi
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 531 - 534
反应条件
1: Et3N
2: Na<PhSO2NCl> / H2O
3: PCl5 / 240 - 250 °C
View Scheme
参考文献
Aktaev,N.P. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, p. 1023 - 1027
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, p. 1117 - 1121
