1-(甲基磺酰基)-l-脯氨酸合成路线 (共 2 条)
反应条件
trifluoroacetic acid in dichloromethane T=23°C; 0.5 h;
参考文献
Costanzo, Michael J.; Yabut, Stephen C.; Almond Jr., Harold R.; Andrade-Gordon, Patricia; Corcoran, Thomas W.; De Garavilla, Lawrence; Kauffman, Jack A.; Abraham, William M.; Recacha, Rosario; Chattopadhyay, Debashish; Maryanoff, Bruce E.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 18 p. 3865 - 3876
反应条件
1: 87 percent / triethylamine / CH2Cl2 / 5 °C 2: 22 percent / trifluoroacetic acid / CH2Cl2 / 0.5 h / 23 °C View Scheme
参考文献
Costanzo, Michael J.; Yabut, Stephen C.; Almond Jr., Harold R.; Andrade-Gordon, Patricia; Corcoran, Thomas W.; De Garavilla, Lawrence; Kauffman, Jack A.; Abraham, William M.; Recacha, Rosario; Chattopadhyay, Debashish; Maryanoff, Bruce E.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 18 p. 3865 - 3876