2-(4-异丁基苯基)-1-丙醇合成路线 （共 19 条）
反应条件
dimethylsulfide borane complex in diethyl ether T=0°C;
参考文献
Galletti, Paola; Emer, Enrico; Gucciardo, Gabriele; Quintavalla, Arianna; Pori, Matteo; Giacomini, Daria
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 18 p. 4117 - 4123
反应条件
methanol; Na-SG in tetrahydrofuran T=0 - 25°C; Bouveault-Blanc reduction; Inert atmosphere;
参考文献
Bodnar, Brian S.; Vogt, Paul F.
Journal of Organic Chemistry, 2009 , vol. 74, # 6 p. 2598 - 2600
反应条件
samarium diiodide; water; triethylamine in tetrahydrofuran T=20°C; 18 h; Inert atmosphere;
参考文献
Szostak, Michal; Spain, Malcolm; Procter, David J.
Organic Letters, 2012 , vol. 14, # 3 p. 840 - 843
反应条件
diisobutylaluminium hydride in diethyl ether; hexane T=-78°C;
参考文献
Chemical Communications, , # 39 p. 4038 - 4040
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0°C; Inert atmosphere; 2: With water; Sodium potassium tartrate in tetrahydrofuran 0.5 h;
参考文献
Friest, Jacob A.; Maezato, Yukari; Broussy, Sylvain; Blum, Paul; Berkowitz, David B.
Journal of the American Chemical Society, 2010 , vol. 132, # 17 p. 5930 - 5931
反应条件
sodium tetrahydroborate; zwitterionic rhodium ν6-tetraphenylborate; isopropyl alcohol in dichloromethane T=100°C; P=25857.4 Torr; 22 h; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 4 p. 233 - 234
反应条件
1: 87 percent / pyridine / CH2Cl2 / 0.5 h / 0 °C 2: 68 percent / K3PO4 / Pd(PPh3)4 / tetrahydrofuran / 18 h / Heating 3: 1.) borane-dimethyl sulfide, 2.) H2O2/NaOH View Scheme
参考文献
Tetrahedron Letters, , vol. 33, # 46 p. 6919 - 6922
反应条件
1: 68 percent / K3PO4 / Pd(PPh3)4 / tetrahydrofuran / 18 h / Heating 2: 1.) borane-dimethyl sulfide, 2.) H2O2/NaOH View Scheme
参考文献
Tetrahedron Letters, , vol. 33, # 46 p. 6919 - 6922
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Roczniki Chemii, , vol. 50, p. 1987 - 1989
反应条件
sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 33, # 46 p. 6919 - 6922
