二乙基2-氯-1,3-薁二羧酸酯合成路线 （共 11 条）
反应条件
1: With hydrogenchloride in benzene 2 h; cooling; 2: With isopentyl nitrite in benzene T=20°C;
参考文献
Chen, Arh-Hwang; Chiu, Shu-Ching; Kuo, Yu-Chen
Synthetic Communications, 2003 , vol. 33, # 15 p. 2701 - 2707
反应条件
1: sodium ethylate; ethanol 2: isopentyl nitrite; benzene; HCl View Scheme
参考文献
McDonald,R.N.; Richmond,J.M.
Journal of Organic Chemistry, 1975 , vol. 40, p. 1689 - 1694
反应条件
1: NaOEt / ethanol 2: HCl, isopentyl nitrite / benzene View Scheme
参考文献
Nozoe et al.
Proceedings of the Japan Academy, 1956 , vol. 32, p. 349,351
反应条件
1: aq. KOH / ethanol 2: 265 - 270 °C 3: aq. KI, AcOH View Scheme
参考文献
Nozoe,T. et al.
Bulletin of the Chemical Society of Japan, 1962 , vol. 35, p. 1990 - 1998
反应条件
1: Na 2: (i) aq. KOH, EtOH, (ii) (pyrolysis) View Scheme
参考文献
Nozoe,T. et al.
Bulletin of the Chemical Society of Japan, 1962 , vol. 35, p. 1990 - 1998
参考文献
Nozoe,T. et al.
Bulletin of the Chemical Society of Japan, 1962 , vol. 35, p. 1990 - 1998
反应条件
in tetrahydrofuran; ammonia
T=-40°C; 1 h;
参考文献
Morita, Tadayoshi; Fujita, Taira; Takase, Kahei
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 6 p. 1647 - 1651
反应条件
ammonium hydroxide in ethanol
参考文献
Nozoe,T. et al.
Bulletin of the Chemical Society of Japan, 1962 , vol. 35, p. 1990 - 1998
反应条件
1: (i) (saponification), (ii) (thermolysis)
2: CCl4
3: (i) aq. KOH, EtOH, (ii) /BRN= 102415/, Et2O
View Scheme
参考文献
McDonald,R.N.; Richmond,J.M.
Journal of Organic Chemistry, 1975 , vol. 40, p. 1689 - 1694
反应条件
1: (i) (saponification), (ii) (thermolysis)
2: CCl4
3: (i) aq. KOH, EtOH, (ii) /BRN= 102415/, Et2O
4: NaH / dimethylformamide
View Scheme
参考文献
McDonald,R.N.; Richmond,J.M.
Journal of Organic Chemistry, 1975 , vol. 40, p. 1689 - 1694
