(3-溴丙基)三苯基溴化磷合成路线 （共 51 条）
反应条件
1: in isopropyl alcohol T=0 - 40°C; 16.25 h; Heating / reflux; 2: With potassium carbonate in water; isopropyl alcohol T=55 - 60°C; P=300.03 Torr; 9 h; Product distribution / selectivity;
参考文献
US2007/232814 A1, ;
Page/Page column 24-25 ;
反应条件
potassium hydride in tetrahydrofuran
-20 deg C to r.t.;
参考文献
Schmidbaur, Hubert; Schier, Annette; Milewski-Mahrla, Beatrix
Chemische Berichte, 1982 , vol. 115, # 2 p. 722 - 731
反应条件
1: (3-bromopropyl)triphenylphosphinium bromide With potassium tert-butylate in tetrahydrofuran
T=70°C; 2 h;
2: 3-phenyl-propionaldehyde in tetrahydrofuran
2 h; Heating;
参考文献
Fuerstner, Alois; Aissa, Christophe
Journal of the American Chemical Society, 2006 , vol. 128, # 19 p. 6306 - 6307
反应条件
1: 83 percent / ethanol / 15 h / 23 °C
2: potassium hexamethyldisilazide / toluene / 1 h / 23 °C
View Scheme
参考文献
Corey, E. J.; Desai, Manoj C.
Tetrahedron Letters, 1985 , vol. 26, # 47 p. 5747 - 5748
反应条件
(i) NaH, (ii) /BRN= 471223/; Multistep reaction;
参考文献
Zhou, Hongwei; Huang, Xian; Chen, Wanli
Synlett, 2003 , # 13 p. 2080 - 2082
反应条件
sodium hydride
1) DME, r.t. 2) DME, 65 deg C, 48 h; Yield given. Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
反应条件
sodium hydride
1) DME, r.t. 2) DME, 75 deg C, 96 h; Yield given. Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
反应条件
sodium hydride
1) DME, r.t. 2) DME, 75 deg C, 96 h; Yield given. Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
反应条件
sodium hydride
1) DME, r.t. 2) DME, 65 deg C, 48 h; Yield given. Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
反应条件
sodium hydride
1) DME, r.t. 2) DME, 65 deg C, 48 h; Yield given. Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
