(3-溴丙基)三苯基溴化磷合成路线 (共 51 条)
反应条件
sodium hydride
1) DME, r.t. 2) DME, 70 deg C, 65 h; Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
反应条件
sodium hydride
1) DME, r.t. 2) DME, 65 deg C, 36 h; Yield given. Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
反应条件
sodium hydride
1) DME, r.t. 2) DME, 68 deg C, 96 h; Yield given. Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
反应条件
sodium hydride
1) DME, r.t. 2) DME, 75 deg C, 48 h; Yield given. Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
反应条件
sodium hydride
1) THF, r.t. 2) THF, 63 deg C, 16 h; Yield given. Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
反应条件
sodium hydride
1) DME, r.t. 2) DME, 80 deg C, 36 h; Yield given. Multistep reaction;
参考文献
Lechevallier, A.; Huet, F.; Conia, J. M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3307 - 3316
反应条件
1: 94 percent / dimethylformamide / 4 h / Heating
2: 92 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
View Scheme
参考文献
Benn, Roger F.; Briggs, Josie C.; McAuliffe, Charles A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 293 - 296
反应条件
1: 100 percent / dimethylformamide / 4 h / Heating
2: 99 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
View Scheme
参考文献
Benn, Roger F.; Briggs, Josie C.; McAuliffe, Charles A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 293 - 296
反应条件
1: 100 percent / dimethylformamide / 4 h / Heating
2: 99 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
3: sulphur / toluene / 2 h
View Scheme
参考文献
Benn, Roger F.; Briggs, Josie C.; McAuliffe, Charles A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 293 - 296
反应条件
potassium tert-butylate in tetrahydrofuran
参考文献
Wang, Bin; Shen, Yu-Mei; Shi, Yian
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9519 - 9521