N-(4-溴苄亚基)-p-甲苯磺酰胺合成路线 (共 10 条)
反应条件
amberlyst 15 in toluene 16 h; HeatingMolecular sieve;
参考文献
Barbarotto, Marie; Geist, Julie; Choppin, Sabine; Colobert, Francoise
Tetrahedron Asymmetry, 2009 , vol. 20, # 24 p. 2780 - 2787
反应条件
1: With 3-keto-2H,3H-1,2-benzisothiazole 1,1-dioxide; lithium bromide in dichloromethane T=20°C; 3 h; 2: in dichloromethane Molecular sieveReflux;
参考文献
Patel, Rajesh; Srivastava, Vishnu P.; Yadav, La Dhar S.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1610 - 1614
反应条件
[bis(acetoxy)iodo]benzene; iodine; sodium acetate in 1,2-dichloro-ethane T=0°C; Inert atmosphere;
参考文献
Li, Weixun; Gan, Jianhong; Fan, Renhua
Tetrahedron Letters, 2010 , vol. 51, # 32 p. 4275 - 4277
反应条件
water; sodium hydrogencarbonate in dichloromethane T=20°C;
参考文献
Thirupathi, Ponnaboina; Kim, Sung Soo
Tetrahedron, 2010 , vol. 66, # 45 p. 8623 - 8628
反应条件
potassium iodide in methanol; water T=25°C; Rate constantMechanism;
参考文献
Knipe, A. C.; McAuley, I. E.; Khandelwal, Y.; Kansal, V. K.
Tetrahedron Letters, 1984 , vol. 25, # 13 p. 1411 - 1414
反应条件
in toluene 20 h; Heating;
参考文献
Naddaka, V. I.; Avanesyan, K. V.; Cherkinskaya, M. L.; Minkin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 6 p. 1154 - 1156
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 6 p. 1282 - 1284
反应条件
(η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate in tetrahydrofuran T=40°C; Mannich type reaction; 30 h; Inert atmosphereMolecular sieve; optical yield given as percent dediastereoselective reaction;
参考文献
Bartoszewicz, Agnieszka; Jezowska, Martina M.; Laymand, Kevin; Moebus, Juri; Martin-Matute, Belen
European Journal of Inorganic Chemistry, 2012 , # 9 p. 1517 - 1530
反应条件
dimethyl sulfoxide T=20°C; Knoevenagel condensation; 2 h; Inert atmosphereMolecular sieve; stereoselective reaction;
参考文献
Chiba, Ryoichi; Oriyama, Takeshi
Chemistry Letters, 2008 , vol. 37, # 12 p. 1218 - 1219
反应条件
FeCl3·6H2O in dichloromethane
T=20°C; Friedel Crafts arylation; 2 h; Inert atmosphere;
参考文献
Thirupathi, Ponnaboina; Soo Kim, Sung
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5240 - 5249
反应条件
in tetrahydrofuran; diethyl ether
T=-5 - 0°C; 0.5 h; Inert atmosphere;
参考文献
Branco, Paula Serio; Raje, Vivek Prabhakar; Dourado, Jorge; Gordo, Joana
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 13 p. 2968 - 2974