N-乙酰-L-苯丙氨酸甲酯合成路线 (共 84 条)
反应条件
triethylamine; zinc dibromide in dichloromethane T=20°C; Solid phase reaction; Acetylation; 24 h; Product distribution; Further Variations:Reagents;
参考文献
Tetrahedron, , vol. 56, # 45 p. 8867 - 8875
反应条件
in chloroform T=23°C; 1 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 50 p. 20318 - 20321
参考文献
Carbohydrate Research, , vol. 22, p. 245 - 256
参考文献
Tetrahedron Letters, , vol. 29, # 19 p. 2295 - 2298
参考文献
Tetrahedron: Asymmetry, , vol. 4, # 6 p. 1137 - 1140
反应条件
hydrazine hydrate in methanol T=20°C; 48 h;
参考文献
Albrecht, Markus; Latorre, Irene; Mehmeti, Gent; Hengst, Konstantin; Oppel, Iris M.
Dalton Transactions, 2011 , vol. 40, # 45 p. 12067 - 12074
反应条件
24 h; Ambient temperature;
参考文献
Xing, Ruye; Hanzlik, Robert P.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 8 p. 1344 - 1351
反应条件
methanol; N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran T=0 - 20°C; Deamination; 0.25 h;
参考文献
Honda, Toshio; Ishikawa, Fumihiro
Chemical Communications, 1999 , # 12 p. 1065 - 1066
反应条件
in acetonitrile T=32°C; 20 h; Irradiation;
参考文献
Deseke, Eckart; Nakatani, Yoichi; Ourisson, Guy
European Journal of Organic Chemistry, 1998 , # 2 p. 243 - 251
反应条件
1: methyl (S)-2-acetamido-3-phenylpropanoate With triphenyl phosphite; chlorine; triethylamine in tetrahydrofuran T=-30°C; 2: 2-methyl-propan-1-ol in tetrahydrofuran T=-30 - 20°C; 3: With water
参考文献
Organic Letters, , vol. 6, # 22 p. 3885 - 3888