2-氨基-4‘-甲基苯甲酮合成路线 （共 42 条）
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Chemische Berichte, , vol. 41, p. 1845
反应条件
CuCl2*H2O; oxygen; potassium carbonate in N,N-dimethyl-formamide T=60°C; 24 h;
参考文献
Zhang, Jintang; Yu, Chenmin; Wang, Sujing; Wan, Changfeng; Wang, Zhiyong
Chemical Communications, 2010 , vol. 46, # 29 p. 5244 - 5246
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.333333 h;
参考文献
Frye, Stephen V.; Johnson, Marty C.; Valvano, Nicole L.
Journal of Organic Chemistry, 1991 , vol. 56, # 11 p. 3750 - 3752
反应条件
1: 60 percent / AlCl3 / CH2Cl2 / 20 °C 2: hydrogen / 10 percent Pd/C / methanol / 6 h / 20 °C / 3750.3 Torr View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 37, # 2 p. 147 - 161
反应条件
1: 60 percent / AlCl3 / CH2Cl2 / 20 °C 2: hydrogen / 10 percent Pd/C / methanol / 6 h / 20 °C / 3750.3 Torr View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 37, # 2 p. 147 - 161
反应条件
aluminium trichloride; phosphorus pentachloride; toluene Erwaermen des Reaktionsprodukts mit Schwefelsaeure;
参考文献
Organic Syntheses, , vol. Coll. Vol. IV, p. 34,35
反应条件
1: PCl5 / 0.5 h / 50 °C 2: AlCl3 3: H2 / 5percent Pd/C / ethanol View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 37, # 1 p. 110 - 115
反应条件
1: 75 percent / triethylamine / aq. ethanol / 1.5 h / Heating 2: 68 percent / n-BuLi / tetrahydrofuran; hexane / 0.33 h / -78 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 56, # 11 p. 3750 - 3752
反应条件
1: 22 percent / aq. Na2CO3 / H2O / 50 - 85 °C 2: 1.) PCl5, 2.) AlCl3 / 1.) 50 deg C, 30 min, 2.) 80 - 90 deg C, 4 h View Scheme
参考文献
Australian Journal of Chemistry, , vol. 43, p. 1547 - 1557
参考文献
Chemische Berichte, , vol. 35, p. 4278
