雌甾-1,3,5(10)-三烯2,3,17-三醇合成路线 （共 26 条）
反应条件
hydrogenchloride in methanol Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 20, p. 1842 - 1843
反应条件
1: 1.) BuLi / 1.) THF, hexane, -78 deg C, 2 h, 2.) THF, hexane, a.) -78 deg C to RT over 2 h, b.) RT, 2 h 2: 55 percent / boron tribromide / CH2Cl2 / 48 h / Ambient temperature View Scheme
参考文献
Australian Journal of Chemistry, , vol. 42, # 3 p. 421 - 432
反应条件
1: KOH 2: Py*HCl / 200 - 220 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 25, p. 585 - 588
反应条件
1: aqueous methanol.KOH 2: BiO3 3: aq.-ethanolic NaOH View Scheme
参考文献
Chemistry and Industry (London, United Kingdom), , p. 1454
Tetrahedron, , vol. 10, p. 144,146
反应条件
1: lead (IV)-acetate 2: aqueous methanol.KOH 3: BiO3 4: aq.-ethanolic NaOH View Scheme
参考文献
Chemistry and Industry (London, United Kingdom), , p. 1454
Tetrahedron, , vol. 10, p. 144,146
反应条件
1: BiO3 2: aq.-ethanolic NaOH View Scheme
参考文献
Chemistry and Industry (London, United Kingdom), , p. 1454
Tetrahedron, , vol. 10, p. 144,146
反应条件
Fremy’s salt; potassium iodide Yield given;
参考文献
Steroids, , vol. 53, # 6 p. 649 - 661
反应条件
hydrogenchloride; sodium periodate; acetic acid
参考文献
Steroids, , vol. 28, # 5 p. 733 - 741
反应条件
1: 70 percent / 48 h / Heating 2: 1.) CCl3F, 2.) Bu4NF / 1.) -78 deg C to 0 deg C, 2.) 25 deg C 3: 12 mg / N-trimethylsilylimidazole / Heating 4: potassium nitrosodisulfonate, KI View Scheme
参考文献
Steroids, , vol. 53, # 6 p. 649 - 661
反应条件
1: 12 mg / N-trimethylsilylimidazole / Heating 2: potassium nitrosodisulfonate, KI View Scheme
参考文献
Steroids, , vol. 53, # 6 p. 649 - 661
