1-苯基-2-丙炔-1-酮合成路线 （共 125 条）
反应条件
(i) LDA, Et2O, (ii) /BRN= 1071220/, THF, (iii) I2; Multistep reaction;
参考文献
Yamada,K. et al.
Synthesis, 1977 , p. 679 - 681
反应条件
(i) LDA, Et2O, (ii) /BRN= 1236431/, THF, (iii) I2; Multistep reaction;
参考文献
Yamada,K. et al.
Synthesis, 1977 , p. 679 - 681
参考文献
Irving; Johnson
Journal of the Chemical Society, 1948 , p. 2037
参考文献
Hoffmann, Siegfried; Hartung, Klaus-Juergen; Hanh, Nguyen thi; Mewes, Reinhard; Baluzow, Wenelin
Zeitschrift fuer Chemie (Stuttgart, Germany), 1986 , vol. 26, # 3 p. 105 - 106
反应条件
in hydrogenchloride; methanol
T=0°C; 0.5 h; microwave irradiation;
参考文献
Bagley, Mark C.; Lubinu, M. Caterina; Mason, Christopher
Synlett, 2007 , # 5 p. 704 - 708
反应条件
triethylamine in methanol
1.) reflux, 0.5 h, 2.) 20 deg C, 6 h;
参考文献
Nakhamanovich, A. S.; Glotova, T. E.; Skvortsova, G. G.; Komarova, T. N.; Skorobogatova, V. I.; Mansurov, Yu. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 6 p. 1221 - 1224
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 6 p. 1371 - 1374
反应条件
1: 38.5 percent / NEt3 / 1.) MeOH, reflux, 0.5 h, 2.) 20 deg C, 6 h, 3.) C6H6, 0 deg C, 2 d
2: N2H4*H2O / ethanol / 1.) reflux, 3 h, 2.) 5 deg C, 1 d
View Scheme
参考文献
Nakhamanovich, A. S.; Glotova, T. E.; Skvortsova, G. G.; Komarova, T. N.; Skorobogatova, V. I.; Mansurov, Yu. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 6 p. 1221 - 1224
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 6 p. 1371 - 1374
反应条件
in methanol
24 h; Ambient temperature;
参考文献
Liso, Gaetano; Trapani, Giuseppe; Reho, Antonia; Latrofa, Andrea; Loiodice, Fulvio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 567 - 572
反应条件
in methanol
3 h; Heatingother alkynes under various react ion conditions; Product distributionMechanism;
参考文献
Liso, Gaetano; Trapani, Giuseppe; Reho, Antonia; Latrofa, Andrea; Loiodice, Fulvio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 567 - 572
反应条件
in methanol
T=20°C; 2 h;
参考文献
Glotova, T. E.; Nakhmanovich, A. S.; Sigalov, M. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # l p. 568 - 571
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 5 p. 680 - 682
