1-苯基-2-丙炔-1-酮合成路线 （共 125 条）
反应条件
N-bromosuccinmide; silver nitrate in acetone
T=20°C; 2 h;
参考文献
Poulsen, Thomas B.; Bernardi, Luca; Aleman, Jose; Overgaard, Jacob; Jorgensen, Karl Anker
Journal of the American Chemical Society, 2007 , vol. 129, # 2 p. 441 - 449
反应条件
1: pyrrole With potassium hydroxide in dimethyl sulfoxide
T=20°C; 0.5 h;
2: carbon disulfide in dimethyl sulfoxide
T=20°C; 2 h;
3: 1-phenyl-prop-2-yne-1-one in dimethyl sulfoxide
2 h;
参考文献
Sobenina; Demenev; Mikhaleva; Elokhina; Stepanova; Mal'kina; Ushakov; Trofimov
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 4 p. 547 - 551
反应条件
1: 82 percent / HClO4 / acetic acid / 3 h / 20 °C
2: 88 percent / NaOH / dimethylsulfoxide / 1 h / 10 - 20 °C
View Scheme
参考文献
Glotova; Protsuk; Albanov; Nakhmanovich; Lopyrev
Russian Journal of General Chemistry, 2003 , vol. 73, # 5 p. 789 - 793
反应条件
in acetic acid
T=20°C; 1 h;
参考文献
Glotova, T. E.; Nakhmanovich, A. S.; Mabarakshina, N. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , p. 578 - 581
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , vol. 24, # 5 p. 705 - 708
反应条件
(i) Et3N, CH2Cl2, (ii) oxalic acid, AcOH; Multistep reaction;
参考文献
Schulz,G. et al.
Chemische Berichte, 1979 , vol. 112, p. 3221 - 3236
