1-苯基-2-丙炔-1-酮合成路线 （共 125 条）
反应条件
1: sodium methoxide / diethyl ether / 5 h / 0 °C 2: 70.5 percent Chromat. / NaBH4, CoCl2 / methanol / 3 h / Ambient temperature; other metal halide, reagents ratio View Scheme
参考文献
Nishio, Takehiko; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 934 - 938
反应条件
potassium carbonate in tetrahydrofuran Ambient temperatureovernight;
参考文献
Hachiken, Hiroko; Takemura, Shoji; Ikeda, Masazumi
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 327 - 331
反应条件
sodium carbonate in acetonitrile T=120°C; 0.666667 h; microwave irradiation;
参考文献
Bagley, Mark C.; Hughes, David D.; Taylor, Paul H.
Synlett, 2003 , # 2 p. 259 - 261
参考文献
Truce,W.E.; Wolf,G.C.
Journal of the Chemical Society [Section] D: Chemical Communications, 1969 , p. 150
反应条件
triethylamine in benzene T=20°C; Yield given. Yields of byproduct given;
参考文献
Bianchi, Giorgio; Gandolfi, Remo; Micheli, Carlo De
Journal of Chemical Research, Miniprint, 1981 , # 1 p. 135 - 158
参考文献
Truce; Heine
Journal of the American Chemical Society, 1957 , vol. 79, p. 5311,5313
参考文献
Bowden; Braude; Jones
Journal of the Chemical Society, 1946 , p. 948
反应条件
1: 1-phenyl-prop-2-yne-1-one With zinc dibromide; lithium diisopropyl amide in tetrahydrofuran; hexane T=-78°C; 0.166667 h; 2: iodobenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=23°C; Further stages.;
参考文献
Anastasia; Negishi Ei
Organic letters, 2001 , vol. 3, # 20 p. 3111 - 3113
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate in water; N,N-dimethyl-formamide T=20°C;
参考文献
Radhakrishnan, Ukkiramapandian; Stang, Peter J.
Organic Letters, 2001 , vol. 3, # 6 p. 859 - 860
反应条件
in water T=150°C; 2 h; High pressureSealed tube;
参考文献
Journal of Organic Chemistry, , vol. 78, # 5 p. 1949 - 1954
