1-苯基-2-丙炔-1-酮合成路线 (共 125 条)
反应条件
in methanol 3 h; Heating;
参考文献
Andriyankova, L. V.; Komarova, T. N.; Nakhmanovich, A. S.; Abramova, N. D.; Skvortsova, G. G.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 12 p. 2388 - 2390
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 12 p. 2610 - 2613
反应条件
1: 82 percent / neutral Al2O3 / CH2Cl2 / 5 h 2: 90 percent / HgO, HBF4 / tetrahydrofuran; H2O / 2 h / Ambient temperature View Scheme
参考文献
Ranu, Brindaban C.; Bhar, Sanjay; Chakraborti, Ratna
Journal of Organic Chemistry, 1992 , vol. 57, # 28 p. 7349 - 7352
反应条件
ethanol; sodium ethanolate T=0 - 5°C;
参考文献
Bowden; Braude; Jones
Journal of the Chemical Society, 1946 , p. 948
反应条件
zinc dibromide in toluene 6 h; Heating;
参考文献
Bagley, Mark C.; Fusillo, Vincenzo; Jenkins, Robert L.; Lubinu, M. Caterina; Mason, Christopher
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1957 - 1968
反应条件
ammonium acetate in ethanol Bohlmann-Rahtz reaction; 24 h; Heating;
参考文献
Xiong, Xin; Bagley, Mark C.; Chapaneri, Krishna
Tetrahedron Letters, 2004 , vol. 45, # 32 p. 6121 - 6124
反应条件
1: 85 percent / ethanol / 1 h / 50 °C 2: 98 percent / N-iodosuccinimide / ethanol / 1 h / 0 °C View Scheme
参考文献
Bagley, Mark C.; Brace, Christian; Dale, James W.; Ohnesorge, Maren; Phillips, Nathan G.; Xiong, Xin; Bower, Justin
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 14 p. 1663 - 1671
反应条件
in acetonitrile 3 h; Heating;
参考文献
Komarova, T. N.; Nakhmanovich, A. S.; Sigalov, M. V.; Glotova, T. E.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 5.2 p. 1058 - 1060
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 5 p. 1176 - 1179
反应条件
phosphorus pentachloride in diethyl ether; dichloromethane Ambient temperature;
参考文献
Naser-Ud-Din; Skattebol, Lars
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 3 p. 247 - 248
反应条件
acetic acid; lithium chloride 26 h; Ambient temperature;
参考文献
Ma, Shengming; Lu, Xiyan; Li, Zhigang
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 709 - 713
反应条件
in acetonitrile T=20°C; 3 h; other α-acetylenic ketones and thiosemicabazone;
参考文献
Komarova, T. N.; Aleksandrova, A. E.; Nakhmanovich, A. S.; Shchegoleva, R. A.; Vinogradova, T. I.
Pharmaceutical Chemistry Journal, 1989 , vol. 23, # 12 p. 1008 - 1009
Khimiko-Farmatsevticheskii Zhurnal, 1989 , vol. 23, # 12 p. 1481 - 1482