1-苯基-2-丙炔-1-酮合成路线 （共 125 条）
反应条件
1: With triphenylphosphine in acetonitrile
T=20°C; 0.5 h; Inert atmosphere;
2: With hydrogenchloride in water; acetonitrile
0.0833333 h; Inert atmosphere;
参考文献
Khong, San; Kwon, Ohyun
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8257 - 8267,11
反应条件
in various solvent(s)
T=250°C; 6 h;
参考文献
Consonni, Roberto; Dalla Croce, Piero; Ferraccioli, Raffaella; La Rosa, Concetta
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 15 p. 1809 - 1814
反应条件
hydroxylamine hydrochloride; sodium carbonate in ethanol
15 h; Heating; Title compound not separated from byproducts;
参考文献
Falorni, Massimo; Lardicci, Luciano; Giacomelli, Giampaolo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 1 p. 7 - 10
反应条件
hydroxylamine hydrochloride; sodium carbonate in ethanol
15 h; Heating; Title compound not separated from byproducts;
参考文献
Falorni, Massimo; Lardicci, Luciano; Giacomelli, Giampaolo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 1 p. 7 - 10
参考文献
Bowden; Jones
Journal of the Chemical Society, 1946 , p. 953
反应条件
4-(N,N-dimethlyamino)pyridine; acetylacetone in dichloromethane
T=20°C; 2 h;
参考文献
Zhou, Qing-Fa; Yang, Fei; Guo, Qing-Xiang; Xue, Song
Synlett, 2007 , # 2 p. 215 - 218
反应条件
CpCo(S2C2B10H8)(CH=CHCO2Me)2 in toluene
T=110°C; 12 h; Schlenk techniqueInert atmosphere; Overall yield = 50 percent;
参考文献
Tang, Xiao; Wang, Zhaojin; Li, Yizhi; Yan, Hong
Journal of Organometallic Chemistry, 2013 , vol. 747, p. 90 - 97
反应条件
in water
T=150°C; P=3600.36 Torr; 2 h; Sealed tube;
参考文献
Iwado, Tatsuya; Hasegawa, Keiya; Sato, Toshiyuki; Okada, Masaki; Sue, Kiwamu; Iwamura, Hiizu; Hiaki, Toshihiko
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1949 - 1954
反应条件
4-(N,N-dimethlyamino)pyridine; acetylacetone in dichloromethane
T=20°C;
参考文献
Zhou, Qing-Fa; Yang, Fei; Guo, Qing-Xiang; Xue, Song
Synlett, 2007 , # 2 p. 215 - 218
反应条件
4-(N,N-dimethlyamino)pyridine; acetylacetone in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Hu, Bin; Zhou, Qing-Fa; Tang, Kai; Xue, Song
Letters in Organic Chemistry, 2009 , vol. 6, # 7 p. 560 - 563
