1-苯基-2-丙炔-1-酮合成路线 （共 125 条）
反应条件
4-(N,N-dimethlyamino)pyridine; acetylacetone in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Hu, Bin; Zhou, Qing-Fa; Tang, Kai; Xue, Song
Letters in Organic Chemistry, 2009 , vol. 6, # 7 p. 560 - 563
反应条件
4-(N,N-dimethlyamino)pyridine; acetylacetone in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Hu, Bin; Zhou, Qing-Fa; Tang, Kai; Xue, Song
Letters in Organic Chemistry, 2009 , vol. 6, # 7 p. 560 - 563
反应条件
4-(N,N-dimethlyamino)pyridine; acetylacetone in dichloromethane
T=20°C; 4 h;
参考文献
Zhou, Qing-Fa; Yang, Fei; Guo, Qing-Xiang; Xue, Song
Synlett, 2007 , # 2 p. 215 - 218
反应条件
4-(N,N-dimethlyamino)pyridine; acetylacetone in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Hu, Bin; Zhou, Qing-Fa; Tang, Kai; Xue, Song
Letters in Organic Chemistry, 2009 , vol. 6, # 7 p. 560 - 563
反应条件
1: 4-nitrobenzaldehdye; methyl amino(3-chlorophenyl)acetate With (Ra)-2,6-di(anthracen-9-yl)-4-hydroxydinaphtho[1,3,2]dioxaphosphepine 4-oxide in toluene
T=50°C; 0.333333 h; Molecular sieve;
2: 1-phenyl-prop-2-yne-1-one in toluene
T=50°C; 60 h; Molecular sieve; Overall yield = 32 percent; enantioselective reaction;
参考文献
Shi, Feng; Xing, Gui-Juan; Tan, Wei; Zhu, Ren-Yi; Tu, Shujiang
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 9 p. 1482 - 1489
反应条件
diethylamine; N,N-dimethyl-formamide in toluene
24 h; Heating;
参考文献
Matsuda, Kenji; Nakamura, Nobuo; Iwamura, Hiizu
Chemistry Letters, 1994 , # 9 p. 1765 - 1768
反应条件
in water
T=150°C; 2 h; High pressureSealed tube;
参考文献
Iwado, Tatsuya; Hasegawa, Keiya; Sato, Toshiyuki; Okada, Masaki; Sue, Kiwamu; Iwamura, Hiizu; Hiaki, Toshihiko
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1949 - 1954
反应条件
sodium in diethyl ether
参考文献
Vereshchagin,L.I. et al.
Journal of Organic Chemistry USSR (English Translation), 1977 , vol. 13, p. 1702 - 1707
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, p. 1836 - 1841
反应条件
monotrimethylsilyl-protected m-phenylenebis(ethynyl)ketone; diethylamine in toluene
参考文献
Matsuda, Kenji; Inoue, Katsuya; Koga, Noboru; Nakamura, Nobuo; Iwamura, Hiizu
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1994 , vol. 253, p. 33 - 40
反应条件
in water
T=150°C; 2 h; High pressureSealed tube;
参考文献
Iwado, Tatsuya; Hasegawa, Keiya; Sato, Toshiyuki; Okada, Masaki; Sue, Kiwamu; Iwamura, Hiizu; Hiaki, Toshihiko
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1949 - 1954
