3,3-二乙氧基-1-苯基丙烷-1-酮合成路线 （共 12 条）
反应条件
trimethylsilyl iodide in dichloromethane T=-78°C; 1 h;
参考文献
Sakurai, Hideki; Sasaki, Koshi; Hosomi, Akira
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 10 p. 3195 - 3196
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=-78°C;
参考文献
Mock, William L.; Tsou, Hwei-Ru
Journal of Organic Chemistry, 1981 , vol. 46, # 12 p. 2557 - 2561
反应条件
in ethanol T=35 - 40°C; 3 h;
参考文献
Vereshchagin, L. I.; Kirillova, L. P.; Luzgina, G. M.; Gareev, G. A.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 4 p. 806 - 808
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 4 p. 886 - 889
反应条件
silica gel in benzene Yield given;
参考文献
Takahashi, Kazumasa; Urano, Yuko; Ogura, Katsuyuki; Iida, Hirotada
Synthesis, 1985 , # 6/7 p. 690 - 691
反应条件
1: 1.) lithium diisopropylamide / HMPT, THF, 1.) -78 deg C, 30 min, 2.) -78 deg C, 30 min, room temp., 3h 2: silica gel / benzene View Scheme
参考文献
Takahashi, Kazumasa; Urano, Yuko; Ogura, Katsuyuki; Iida, Hirotada
Synthesis, 1985 , # 6/7 p. 690 - 691
反应条件
1: 1.) lithium diisopropylamide / HMPT, THF, 1.) -78 deg C, 30 min, 2.) -78 deg C, 30 min, room temp., 3h 2: silica gel / benzene View Scheme
参考文献
Takahashi, Kazumasa; Urano, Yuko; Ogura, Katsuyuki; Iida, Hirotada
Synthesis, 1985 , # 6/7 p. 690 - 691
反应条件
ethanol; sodium ethanolate T=0 - 5°C;
参考文献
Bowden; Braude; Jones
Journal of the Chemical Society, 1946 , p. 948
反应条件
1: Et3N 2: 83 percent / zinc chloride / ethyl acetate / 3 h / 20 - 25 °C View Scheme
参考文献
Makin, S. M.; Kruglikova, R. I.; Popova, T. P.; Tagirov, T. K.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 4 p. 630 - 634
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 4 p. 723 - 727
反应条件
perchloric acid 10 h; Ambient temperature;
参考文献
Pikus, A. L.; Feigel'man, V. M.; Mezheritskii, V. V.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 12.2 p. 2333 - 2337
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 12 p. 2603 - 2608
反应条件
1: ZnI2 2: (i) LDA, THF, Et2O, (ii) /BRN= 635754/, (iii) (hydrolysis) View Scheme
参考文献
Deuchert,K. et al.
Chemische Berichte, 1979 , vol. 112, p. 2045 - 2061
