3,4,5-三甲氧基苯基原醇甲酯合成路线 （共 7 条）
反应条件
iodine; magnesium in methanol T=20°C; 0.5 h;
参考文献
Khurana, Jitender M.; Bansal, Geeti; Kukreja, Gagan; Pandey, Ravi R.
Monatshefte fur Chemie, 2003 , vol. 134, # 10 p. 1365 - 1371
反应条件
1: T=0 - 20°C; 8 h; Inert atmosphere; 2: With water in diethyl ether Inert atmosphere;
参考文献
Tanpure, Rajendra P.; Harkrider, Amanda R.; Strecker, Tracy E.; Hamel, Ernest; Trawick, Mary Lynn; Pinney, Kevin G.
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 19 p. 6993 - 7001
反应条件
in diethyl ether T=0 - 5°C; Grignard reaction; 2 h;
参考文献
Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 1 p. 251 - 268
反应条件
copper(l) iodide; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; potassium tert-butylate; L-proline in N,N-dimethyl-formamide T=25°C; 5 h;
参考文献
Zhang, Guofu; Han, Xingwang; Luan, Yuxin; Wang, Yong; Wen, Xin; Ding, Chengrong
Chemical Communications, 2013 , vol. 49, # 72 p. 7908 - 7910
反应条件
4-chloro-1-ethenylbenzene; [N,N'-bis(2-(2-adamantyl)oxycarbonyl-3-oxobutylidene)-(1S,2S)-dimesitylethylenediaminato]cobalt(II); oxygen in tert-butyl alcohol T=20 - 50°C; Resolution of racemate; optical yield given as percent ee;
参考文献
Yamada, Tohru; Higano, Sho; Yano, Takanori; Yamashita, Yoshihiro
Chemistry Letters, 2009 , vol. 38, # 1 p. 40 - 41
反应条件
trichlorophosphate Condensation; 3 h; Heating;
参考文献
Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 1 p. 251 - 268
反应条件
1: copper(l) iodide; 1,10-phenanthroline; potassium phosphate / 1,4-dioxane / 80 °C / |Schlenk technique
2: sodium hydride / toluene / 12 h / 65 °C / |Inert atmosphere
View Scheme
参考文献
Reddy, Alavala Gopi Krishna; Mahendar, Lodi; Satyanarayana, Gedu
Synthetic Communications, 2014 , vol. 44, # 14 p. 2076 - 2087
