1: 76.5 percent / dichlorobis(triphenylphosphine)nickel (II) / tetrahydrofuran / 24 h / Ambient temperature
2: acetone / 20 h / 100 °C / in high pressure vessel
3: H2 / 5percent PtO2/C / methanol / 24 h / Ambient temperature
4: 75 percent / 48percent HBr / 4 h / 120 °C
View Scheme
C54H80Cl2Fe2N2O4 in diethyl ether
T=22°C; 0.5 h; Inert atmosphere;
参考文献
UNIVERSITY OF PRINCE EDWARD ISLAND; GENESIS GROUP INC.; SHAVER, Michael, P.; KOZAK, Christopher, M.
Patent: WO2013/53046 A1, 2013 ;
Location in patent: Paragraph 00187-00191 ;