反应条件
1: DIBAL-H / hexamethylphosphoric acid triamide; tetrahydrofuran / 1.) 0 deg C, 1 h; 2.) 25 deg C, 16 h
2: NaOH / H2O; ethanol / 1 h / Heating
3: benzoquinone, MnO2 / Pd(OAc)2 / tetrahydrofuran
View Scheme
参考文献
Minami, Toru; Hirakawa, Kazunari; Koyanagi, Shinichiro; Nakamura, Seigo; Yamaguchi, Masahiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2385 - 2390
