1,3,5-三氟-2,4,6-三甲基苯合成路线 (共 9 条)
反应条件
hydrogenchloride; sodium tetrafluoroborate; sodium nitrite Erhitzen des Reaktionsprodukts;
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: iron 2: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts 3: hydrogen fluoride; sodium nitrate 4: iron 5: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: hydrogen fluoride; sodium nitrate 2: iron 3: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: aqueous hydrochloric acid; sodium nitrite; aqueous sodium-tetrafluoroborate / Erhitzen des Reaktionsprodukts 2: iron 3: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts 4: hydrogen fluoride; sodium nitrate 5: iron 6: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts 2: hydrogen fluoride; sodium nitrate 3: iron 4: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
1: iron 2: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts View Scheme
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
potassium hydroxide 1.) NH3(l), -40 degC, 1 h, 2.) 20 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Shtark, A. A.; Chuikova, T. V.; Shteingarts, V. D.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 5 p. 960 - 967
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 5 p. 1055 - 1063
反应条件
tetrachloromethane; chlorine T=200°C; Photolysis;
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98
反应条件
tetrachloromethane; chlorine
Licht einer 200 W-Lampe;
参考文献
Finger et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 153
Journal of the American Chemical Society, 1959 , vol. 81, p. 94,98