反应条件
in diethyl ether addn. of Ag(CF3CO2) to a soln. of Li(C6F5) in diethyl ether at -78°C, stirred for 60 min under N2, addn. of (P(C6H5)(CH3)3)(CF3CO2), stirred for 10 min, warmed to room temp.; pptn. filtered off, washed with water, dissolved in diethyl ether, filtered through a layer of anhydrous MgSO4, evapd., addn. of n-hexane, pptn.; elem. anal.;
参考文献
Uson, Rafael; Laguna, Antonio; Uson, Alfredo; Jones, Peter G.; Meyer-Baese, Karen
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 341 - 346
