1: With n-butyllithium in diethyl ether T=-70°C; 1 h; 2: With tellurium in diethyl ether T=-70 - 25°C; 1.5 h; 3: With iodine in diethyl ether T=25°C; 0.25 h;
参考文献
Klapoetke, Thomas M.; Krumm, Burkhard; Mayer, Peter; Polborn, Kurt; Ruscitti, Oliver P.
Journal of Fluorine Chemistry, 2001 , vol. 112, # 2 p. 207 - 212
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1.5 h; 2: With tellurium; tributylphosphine in tetrahydrofuran; hexane T=-20°C; 15 h; 3: With iodine in tetrahydrofuran; hexane 2 h; Heating;
参考文献
Klapoetke, Thomas M.; Krumm, Burkhard; Mayer, Peter; Naumann, Dieter; Schwab, Ingo
Journal of Fluorine Chemistry, 2004 , vol. 125, # 6 p. 997 - 1005
