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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
五氟苯
合成路线
（共 532 条）
363-72-4
五氟苯
+
369-57-3
四氟硼酸重氮苯盐
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
反应条件
potassium phosphate; copper(l) iodide; 1,10-phenanthroline; tetra-(n-butyl)ammonium iodide in dimethyl sulfoxide; acetonitrile T=130°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Zhu, Xingyi; Li, Feng; Su, Weike
Tetrahedron Letters, 2013 , vol. 54, # 10 p. 1285 - 1289
363-72-4
五氟苯
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
反应条件
palladium diacetate; silver(l) oxide in 1-methyl-pyrrolidin-2-one T=100°C; 15 h; GloveboxSchlenk technique;
参考文献
Fang, Xin; Huang, Yuanyuan; Chen, Xiaoqing; Lin, Xiaoxi; Bai, Zhengshuai; Huang, Kuo-Wei; Yuan, Yaofeng; Weng, Zhiqiang
Journal of Fluorine Chemistry, 2013 , vol. 151, p. 50 - 57
363-72-4
五氟苯
+
74497-02-2
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
反应条件
1: aniline With tert.-butylnitrite; boron trifluoride diethyl etherate in tetrahydrofuran T=-15 - 20°C; Schlenk techniqueInert atmosphere; 2: 2,3,4,5,6-pentafluorobenzene With potassium phosphate; copper(l) iodide; 1,10-phenanthroline; tetra-(n-butyl)ammonium iodide in dimethyl sulfoxide; acetonitrile T=130°C; 4 h; Schlenk technique;
参考文献
Zhu, Xingyi; Li, Feng; Su, Weike
Tetrahedron Letters, 2013 , vol. 54, # 10 p. 1285 - 1289
363-72-4
五氟苯
+
108-90-7
氯苯
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium carbonate in isopropanol acetate T=80°C; 12 h;
参考文献
Lafrance, Marc; Shore, Daniel; Fagnou, Keith
Organic Letters, 2006 , vol. 8, # 22 p. 5097 - 5100
363-72-4
五氟苯
+
17763-67-6
苯基三氟甲烷磺酸酯
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium carbonate in isopropanol acetate T=80°C; 12 h;
参考文献
Lafrance, Marc; Shore, Daniel; Fagnou, Keith
Organic Letters, 2006 , vol. 8, # 22 p. 5097 - 5100
363-72-4
五氟苯
+
98-80-6
苯硼酸
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
反应条件
palladium diacetate; potassium carbonate; 4-methyl-benzoic acid; silver carbonate in dimethylammonium 2,4-dichlorophenoxyacetate T=110°C; 10 h;
参考文献
Wei, Ye; Kan, Jian; Wang, Min; Su, Weiping; Hong, Maochun
Organic Letters, 2009 , vol. 11, # 15 p. 3346 - 3349
108-86-1
溴代苯
+
363-72-4
五氟苯
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in toluene T=80°C; 3 h; Inert atmosphereSchlenk technique;
参考文献
Ma, Xiaowei; Liu, Yan; Liu, Ping; Xie, Jianwei; Dai, Bin; Liu, Zhiyong
Applied Organometallic Chemistry, 2014 , vol. 28, # 3 p. 180 - 185
363-72-4
五氟苯
+
873-55-2
苯亚磺酸钠
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
反应条件
Na3PO4*12H2O; silver carbonate; palladium dichloride in water; dimethyl sulfoxide T=100°C; 18 h; Schlenk technique; Reagent/catalystTime;
参考文献
Miao, Tao; Wang, Lei
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 2-3 p. 429 - 436
363-72-4
五氟苯
+
16156-59-5
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium carbonate in toluene; tert-butyl alcohol T=120°C; 17 h; Inert atmosphereMicrowave irradiation;
参考文献
Chang, Joyce Wei Wei; Chia, Eugene Yurong; Chai, Christina Li Lin; Seayad, Jayasree
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 11 p. 2289 - 2299
106-38-7
+
363-72-4
五氟苯
→
反应条件
784-14-5
2,3,4,5,6-五氟联苯
+
14621-04-6
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in toluene T=80°C; 3 h; Inert atmosphereSchlenk technique; Reagent/catalystSolvent; Overall yield = 95 percent;
参考文献
Ma, Xiaowei; Liu, Yan; Liu, Ping; Xie, Jianwei; Dai, Bin; Liu, Zhiyong
Applied Organometallic Chemistry, 2014 , vol. 28, # 3 p. 180 - 185
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