1,2-O-双十四烷基-rac-甘油合成路线 (共 5 条)
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate P=2585.81 Torr; 12 h;
参考文献
Kasireddy, Krishnudu; Ahmad, Moghis U.; Ali, Shoukath M.; Ahmad, Imran
Tetrahedron Letters, 2004 , vol. 45, # 13 p. 2743 - 2746
反应条件
methanol; sodium tetrahydroborate T=25°C; 6 h;
参考文献
Roy; Letellier; Fenske; Jarrell
Journal of the Chemical Society - Series Chemical Communications, 1990 , # 5 p. 378 - 380
反应条件
1: 79 percent / NaH / dimethylformamide / 16 h / 20 - 60 °C 2: 89 percent / hydrogen / Pd/C / ethyl acetate / 4 h / 2585.81 Torr View Scheme
参考文献
Bioorganic Chemistry, , vol. 33, # 5 p. 345 - 362
反应条件
1: 88 percent / H5IO6 / diethyl ether / 20 h / 25 °C 2: 93 percent / NaBH4, MeOH / 6 h / 25 °C View Scheme
参考文献
Journal of the Chemical Society - Series Chemical Communications, , # 5 p. 378 - 380
反应条件
1: 91 percent / 1 M HCl / methanol; CHCl3 / 96 h / Heating 2: 88 percent / H5IO6 / diethyl ether / 20 h / 25 °C 3: 93 percent / NaBH4, MeOH / 6 h / 25 °C View Scheme
参考文献
Journal of the Chemical Society - Series Chemical Communications, , # 5 p. 378 - 380