5,5-二氟-1-甲基-1,5-二氢-2H-吡咯-2-酮合成路线 （共 7 条）
反应条件
1: With Et3N-5HF in acetonitrile T=20°C; Electrochemical reaction; 2: With water in acetonitrile 4 h;
参考文献
Tajima, Toshiki; Nakajima, Atsushi; Fuchigami, Toshio
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1436 - 1441
反应条件
triethylamine tris(hydrogen fluoride) in acetonitrile T=20°C; Electrochemical reaction;
参考文献
Tajima, Toshiki; Nakajima, Atsushi; Fuchigami, Toshio
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1436 - 1441
反应条件
Et3N-5HF; water in acetonitrile T=20°C; Electrochemical reaction;
参考文献
Tajima, Toshiki; Ishii, Hideki; Fuchigami, Toshio
Tetrahedron Letters, 2001 , vol. 42, # 29 p. 4857 - 4860
反应条件
1: 20 percent Spectr. / Et3N*2HF / 1,2-dimethoxy-ethane / 20 °C / Electrochemical reaction 2: 66 percent Spectr. / Et3N*3HF / acetonitrile / 20 °C / Electrochemical reaction 3: 83 percent Spectr. / H2O / acetonitrile / 4 h View Scheme
参考文献
Tajima, Toshiki; Ishii, Hideki; Fuchigami, Toshio
Tetrahedron Letters, 2001 , vol. 42, # 29 p. 4857 - 4860
反应条件
water in acetonitrile 4 h;
参考文献
Tajima, Toshiki; Ishii, Hideki; Fuchigami, Toshio
Tetrahedron Letters, 2001 , vol. 42, # 29 p. 4857 - 4860
反应条件
1: 66 percent Spectr. / Et3N*3HF / acetonitrile / 20 °C / Electrochemical reaction 2: 83 percent Spectr. / H2O / acetonitrile / 4 h View Scheme
参考文献
Tajima, Toshiki; Ishii, Hideki; Fuchigami, Toshio
Tetrahedron Letters, 2001 , vol. 42, # 29 p. 4857 - 4860
反应条件
triethylamine tris(hydrogen fluoride) in acetonitrile T=20°C; Electrolysis; Product distribution; Further Variations:Reagents;
参考文献
Tajima, Toshiki; Fuchigami, Toshio
Synthesis, 2002 , # 17 p. 2597 - 2600
